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Characterization of Tantalum Oxide Thin Films Prepared by Cylindrical Magnetron Sputtering: Influence of O2% in the Gas Mixture

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Abstract

The amorphous tantalum oxide thin films were prepared by DC reactive magnetron cylindrical sputtering onto p-type silicon (100) substrate. We report the composition and optical properties of thin films under O2 amount variation. The sample’s reflectance was measured with a UV-Vis-NIR spectrophotometer (320–850 nm). The optical characterization of thin layers was analyzed by ellipsometry in spectral region for wavelength from 250 to 850 nm to obtain the refractive index and film’s thickness. The RMS roughness and grain size were investigated by atomic force microscope (AFM). Simulations to Rutherford backscattering spectroscopy (RBS) data revealed film’s stoichiometry. The reflectance, refractive index, thickness, RMS roughness and grain size were found to be affected by increasing oxygen amount. We calculated the porosity of grown layers using measured refractive index at the wavelength of 633 nm.

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References

  1. F. Rubio, J.M. Albella, J. Denis, J.M. Martinz-Duart, J. Vac. Sci. Technol. 21, 1043 (1982)

    Article  ADS  Google Scholar 

  2. E.G. Farhd, Z.T. Fatma, G.T. Gali, Thin Solid Films 295, 11–15 (1997)

    Article  Google Scholar 

  3. W.J. Liu, X.J. Guo, C.H. Chen, Surf. Coat. Technol. 196, 69–75 (2005)

    Article  Google Scholar 

  4. I. Proqueras, J. Marti, E. Bertran, Thin Solid Films 343, 449 (1999)

    Article  ADS  Google Scholar 

  5. Y. Imai, A. Watanabe, M. Mukaida, K. Osato, T. Tsunoda, T. Kameyama, K. Fukuda, Thin Solid Films 261, 76 (1995)

    Article  ADS  Google Scholar 

  6. Nalwa H.S., Handbook of surfaces and interfaces of materials (Academic Press, San Diego, USA, 2001) p. 439

  7. N. Gaillard, L. Pinzelli, M. Gros-Jean, Appl. Phys. Lett. 89, 133506 (2006)

    Article  ADS  Google Scholar 

  8. Z. Todorva, N. Donkov, Z. Ristic, N. Bundaleski, S. Petrovic, M. Petkov, Plasma Process. Polym. 3, 174 (2006)

    Article  Google Scholar 

  9. F.E. Ghodsi, F.Z. Tepehan, Sol. Energ. Mater. Sol. Cell 59, 367–375 (1999)

    Article  Google Scholar 

  10. S. Yidirim, K. Ulutas, D. Deger, E.O. Zayim, I. Turhan, Vacuum 777(3), 329–335 (2005)

    Article  Google Scholar 

  11. G. Marius, H. Wilhelm, K.T. Markus, Thin Solid Films 516(2/4), 136–140 (2007)

    Google Scholar 

  12. S.G. Yoon, H.K. Kim, H.M. Lee, D.H. Yoon, Thin Solid Films 475, 239 (2005)

    Article  ADS  Google Scholar 

  13. Y.-H. Pai, C.-C. Chou, F.-S. Shieu, Mater. Chem. Phys. 107, 524–527 (2008)

    Article  Google Scholar 

  14. E. Franke, M. Schubert, C.L. Trimble, M.J. DeVries, J.A. Woollam, Thin Solid Films 388, 283–289 (2001)

    Article  ADS  Google Scholar 

  15. S.V. Jagadeesh Chandra, C.-J. Choi, S. Uthanna, G. Mohan Rao, Mater. Sci. Semicond. Process. 13, 245–251 (2010)

    Google Scholar 

  16. S.V. Jagadeesh Chandra, S. Uthanna, G. Mohan Rao, Appl. Surf. Sci. 254, 1953–1960 (2008)

    Google Scholar 

  17. J.-c Zhou, D.-t. Luo, Y.-z. Li, Z. Liu, Trans. Nonferrous Metals Soc. China 19, 359–363 (2009)

    Article  Google Scholar 

  18. J.M. Ngaruiya, S. Venkataraj, R. Drese, O. Kappertz, T.P. Leervad Pedersen, M. Wuttig, Phys. Stat. sol. (a). 198, 99–110 (2003)

  19. O. Madelung, M. Schulz, H. Weiss, Landolt-Börstein Semiconductors, Physics of non-tetrahedrally bonded binary compounds III (Springer, Berlin, 1984)

    Google Scholar 

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Correspondence to E. Hassani Sadi.

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Hantehzadeh, M.R., Hassani Sadi, E. & Darabi, E. Characterization of Tantalum Oxide Thin Films Prepared by Cylindrical Magnetron Sputtering: Influence of O2% in the Gas Mixture. J Fusion Energ 31, 374–378 (2012). https://doi.org/10.1007/s10894-011-9478-0

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