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Journal of Chemical Crystallography

, Volume 41, Issue 1, pp 82–84 | Cite as

Microwave Synthesis and Crystal Structure of 2-Hydroxy-3-iodo-benzaldehyde-copper (II)

  • Suo-Ping Xu
  • Xiao-Liang Wang
  • Jian-Feng Tang
  • Ban-Feng Ruan
  • Hai-Liang Zhu
Communication

Abstract

One new complex, 2-hydroxy-3-iodo-benzaldehyde-copper (II) has been designed and microwave synthesized. The structure was determined by UV, IR and single X-ray crystallography study. The title complex C14H8CuI2O4 crystallizes in the orthorhombic space group Pna21 with the cell parameters a = 12.7897(12) Å, b = 6.1132(8) Å, c = 19.5114(18) Å, V = 1525.5(3) Å3 and Z = 4. The central copper (II) is four-coordinated by four oxygen atoms from two 3-iodosalicylaldehyde. The complex is linked into rhombic crystals by weak intermolecular interactions.

Graphical Abstract

One new complex, 2-hydroxy-3-iodo-benzaldehyde-copper (II) has been designed and microwave synthesized. The structure was determined by UV, IR and single X-ray crystallography study.

Keywords

Crystal structure 3-iodosalicylaldehyde Microwave synthesis Copper (II) 

Notes

Acknowledgments

The work was co-financed by grants (Projects 30772627) from National Natural Science Foundation of China and (Projects 09KJD150005) from Natural Science Foundation of Jiangsu Province, China.

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Copyright information

© Springer Science+Business Media, LLC 2010

Authors and Affiliations

  • Suo-Ping Xu
    • 1
    • 2
  • Xiao-Liang Wang
    • 1
  • Jian-Feng Tang
    • 1
  • Ban-Feng Ruan
    • 1
  • Hai-Liang Zhu
    • 1
  1. 1.State Key Laboratory of Pharmaceutical BiotechnologyNanjing UniversityNanjingChina
  2. 2.School of Chemistry and Chemical EngineeringXuzhou Normal UniversityXuzhouChina

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