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Superparamagnetic behaviour of zinc ferrite obtained by the microwave assisted method

  • B. Hangai
  • E. Borsari
  • E. C. Aguiar
  • F. G. Garcia
  • E. Longo
  • A. Z. Simões
Article

Abstract

Magnetic ZnFe2O4 nanoparticles with magnetization saturation of 12.1 emu/g were synthesized through hydrothermal microwave method at 140 °C for 32 min. These compound is being tested in magnetic hyperthermia a promising therapeutic cancer treatment, which causes lysis of tumor cells by heating magnetic nanoparticles through an external magnetic field. X-ray diffraction reveals a single-phase ZnFe2O4 nanoparticles with well-defined structure while Raman spectroscopy reveals that at 32 min of soaking time provides the energy crystallization, causing anisotropy in the structural growth at short range causing a certain degree of order in the crystal lattice. Morphology of the powders was investigated by transmission electronic microscopy (HRTEM) which showed particle sizes with 10–25 nm of diameter being an important factor for application in magneto-hyperthermia. Magnetic parameters analyzed by means of a vibrating-sample magnetometer unit showed that these nanoparticles have great potential in magneto-hyperthermia application.

Keywords

Ferrite ZnFe2O4 Microwave Energy Zinc Ferrite Spinel Ferrite 
These keywords were added by machine and not by the authors. This process is experimental and the keywords may be updated as the learning algorithm improves.

Notes

Acknowledgements

The financial support of this research project by the Brazilian research funding agency FAPESP (2016/02180-4) is gratefully acknowledged.

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Copyright information

© Springer Science+Business Media New York 2017

Authors and Affiliations

  • B. Hangai
    • 1
  • E. Borsari
    • 1
  • E. C. Aguiar
    • 4
  • F. G. Garcia
    • 2
  • E. Longo
    • 3
  • A. Z. Simões
    • 1
  1. 1.Faculty of Engineering of GuaratinguetáSão Paulo State University - UNESPGuaratinguetáBrazil
  2. 2.Physics and Chemistry InstituteFederal University of Itajubá - UNIFEIItajubáBrazil
  3. 3.Interdisciplinary Laboratory of Electrochemistry and Ceramics, LIEC - Department of Chemistry Techonology, Chemistry InstituteSão Paulo State University - UNESPAraraquaraBrazil
  4. 4.Mato Grosso do Sul State UniversityCidade Universitária, UEMSDouradosBrazil

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