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Synthesis and characterization of high quality {100} diamond single crystal

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Abstract

Non-destructive characterization of diamond plate can provide abundant information. Consequently, it will help improve the growth technique. In this paper, unintentionally doped {100} diamond single crystal (type Ib) was synthesized by the temperature gradient growth (TGG) method under high pressure (~6.5 GPa) and high temperature (~1500 °C) condition. The crystal morphology was observed by confocal laser scanning microscope (CLSM). The result indicated there was a pit on diamond surface. UV/Vis transmission measurement indicated the maximum transmittance of our sample was about 9% lower than that of theoretical value. Fourier-transformation infrared spectroscopy (FTIR) measurement confirmed that the nitrogen concentration was about 53 ppm. High resolution X-Ray diffractometer (HRXRD) was employed to evaluated the crystalline quality, and result showed that the full width of half maximum (FWHM) at (400) and (111) rocking curves were 56.9′′, 23.7′′, respectively, which revealed the good crystalline quality. In addition, the diffraction peak of (400) lattice plane exhibited an increase trend with the X-ray beam position, showing the (100) lattice surface was convex bended.

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Acknowledgements

This work was financially supported by “Science and technology project of China State Grid Corp” under Grant SGSDDK00KJJS1600071, Natural Science Foundation of China under Grants (513230013, 61327808) and National Key Research and Development program under Grant 2016YFB0400201.

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Authors and Affiliations

  1. State Key Laboratory of Crystal Materials, Shandong University, Jinan, 250100, China

    Xuejian Xie, Xiwei Wang, Yan Peng, Yingxin Cui, Xiufang Chen, Xiaobo Hu & Xiangang Xu

  2. Collaborative Innovation Center for Global Energy Interconnection (Shandong), Jinan, 250061, China

    Xuejian Xie, Xiwei Wang, Yan Peng, Yingxin Cui, Xiufang Chen, Xiaobo Hu, Xiangang Xu, Peng Yu & Ruiqi Wang

  3. Jinan Zhongwu New Material Co. Ltd, Jinan, 250101, China

    Xiwei Wang

  4. State Grid Shandong Electric Power Research Institute, Jinan, 250001, China

    Peng Yu & Ruiqi Wang

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  1. Xuejian Xie
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  2. Xiwei Wang
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  3. Yan Peng
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Correspondence to Yan Peng or Xiangang Xu.

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Xie, X., Wang, X., Peng, Y. et al. Synthesis and characterization of high quality {100} diamond single crystal. J Mater Sci: Mater Electron 28, 9813–9819 (2017). https://doi.org/10.1007/s10854-017-6735-7

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  • DOI: https://doi.org/10.1007/s10854-017-6735-7

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