Skip to main content

Advertisement

Log in

Tensile and compressive deformation behavior of peak-aged cast Mg–11Y–5Gd–2Zn–0.5Zr (wt%) alloy at elevated temperatures

  • Original Paper
  • Published:
Journal of Materials Science Aims and scope Submit manuscript

Abstract

The tensile and compressive deformation behavior of a peak-aged cast Mg–11Y–5Gd–2Zn–0.5Zr (wt%) (WGZ1152-T6) alloy was investigated at temperatures between 25 and 400 °C (0.33T m–0.75 T m) and strain rate ranges of 1 × 10−4 to 1 × 10−2 s−1. The tensile strength (263 ± 9.5 MPa) and compressive strength (246 ± 9.0 MPa) at 300 °C were 86 and 49 % of those at room temperature (RT), respectively. The alloy showed anomalous positive temperature dependence of tensile strength from RT to 200 °C, while the compressive strength decreased with increasing temperature for all the temperatures studied. The tensile strength and yield stress of the alloy were considerably superior to those of WE54-T6 and AC8A-T6 at 25 to 400 °C. The flow behavior of the alloy can be described by the Garofalo hyperbolic sine constitutive equation at 250–400 °C. For tension, the stress exponent n was 7.7 ± 0.7 and the activation energy of deformation Q was 274 ± 10 kJ/mol; for compression, n was 8.7 ± 0.4 and Q was 367 ± 6 kJ/mol. The values of n and Q indicate that the dislocation cross slip was the rate-controlling mechanism, which was consistent with the observed short wavy slip traces usually associated with cross slip. The alloy exhibited obvious tension–compression yield asymmetry at RT, and the asymmetry reduced significantly with increasing temperature. The deformation microstructure revealed that twinning was most probably responsible for the asymmetry, and the nonbasal slip and cross slip played an important role in the reduced asymmetry at high temperatures.

This is a preview of subscription content, log in via an institution to check access.

Access this article

Price excludes VAT (USA)
Tax calculation will be finalised during checkout.

Instant access to the full article PDF.

Figure 1
Figure 2
Figure 3
Figure 4
Figure 5
Figure 6
Figure 7
Figure 8
Figure 9
Figure 10
Figure 11
Figure 12
Figure 13
Figure 14

Similar content being viewed by others

References

  1. Okamoto K, Sasaki M, Takahashi N, Wang QD, Gao Y, Yin DD, Chen CJ (2011) Applicability of Mg–Zn–(Y, Gd) alloys for engine pistons. In: Sillekens WH, Agnew SR, Neelameggham NR, Mathaudhu SN (eds) Magnesium technology. Wiley, Hoboken, pp 73–78. http://onlinelibrary.wiley.com/book/10.1002/9781118062029

  2. Perez Prado MT, Cepeda Jimenez CM (2015) Strength ceiling smashed for light metals. Nature 528:486–487

    Article  Google Scholar 

  3. Wu ZX, Curtin WA (2015) The origins of high hardening and low ductility in magnesium. Nature 526:62

    Article  Google Scholar 

  4. Yin DD, Wang QD, Boehlert CJ, Janik V (2012) Creep and fracture behavior of peak-aged Mg–11Y–5Gd–2Zn–0.5Zr (wt%). Metall Mater Trans A 43A:3338–3350

    Article  Google Scholar 

  5. Boehlert CJ, Knittel K (2006) The microstructure, tensile properties, and creep behavior of Mg–Zn alloys containing 0–4.4wt.% Zn. Mater Sci Eng A 417:315–321

    Article  Google Scholar 

  6. Pan HC, Ren YP, Fu H, Zhao H, Wang LQ, Meng XY, Qin GW (2016) Recent developments in rare-earth free wrought magnesium alloys having high strength: a review. J Alloy Compd 663:321

    Article  Google Scholar 

  7. He SM, Zeng XQ, Peng LM, Gao X, Nie JF, Ding WJ (2007) Microstructure and strengthening mechanism of high strength Mg–10Gd–2Y–0.5Zr alloy. J Alloy Compd 427:316–323

    Article  Google Scholar 

  8. Chen CJ, Wang QD, Yin DD (2009) Thermal properties of Mg–11Y–5Gd–2Zn–0.5Zr (wt%) alloy. J Alloy Compd 487:560–563

    Article  Google Scholar 

  9. Chen CJ, Wang QD, Yin DD, Ding WJ (2009) Research process in piston materials of combustion engine (in Chinese). Mater Rev 62

  10. Wu GH, Fan Y, Gao HT, Zhai CQ, Zhu YP (2005) The effect of Ca and rare earth elements on the microstructure, mechanical properties and corrosion behavior of AZ91D. Mater Sci Eng A 408:255

    Article  Google Scholar 

  11. Pekguleryuz MO, Kaya AA (2003) Creep resistant magnesium alloys for powertrain applications. Adv Eng Mater 5:866

    Article  Google Scholar 

  12. Xu DK, Han EH (2012) Effects of icosahedral phase formation on the microstructure and mechanical improvement of Mg alloys: a review. Prog Nat Sci Mater 22:364

    Article  Google Scholar 

  13. Kwak TY, Lim HK, Kim WJ (2015) Hot compression characteristics and processing maps of a cast Mg–9.5Zn–2.0Y alloy with icosahedral quasicrystalline phase. J Alloy Compd 644:645–653

    Article  Google Scholar 

  14. Qin QF, Tan YX, Zhang ZM, Wang Q, Yang B (2016) Effects of homogenization on hot deformation behavior of as-cast Mg–8Gd–Y–1Nd–0.5Zr magnesium alloy. J Mater Eng Perform 25:304

    Article  Google Scholar 

  15. Lentz M, Gall S, Schmack F, Mayer HM, Reimers W (2014) Hot working behavior of a WE54 magnesium alloy. J Mater Sci 49:1121–1129. doi:10.1007/s10853-013-7790-y

    Article  Google Scholar 

  16. Zheng XW, Luo AA, Dong J, Sachdev AK, Ding WJ (2012) Plastic flow behavior of a high-strength magnesium alloy NZ30K. Mater Sci Eng A 532:616

    Article  Google Scholar 

  17. Yin DD, Wang QD, Boehlert CJ, Ding WJ (2012) Creep and fracture behavior of as-cast Mg–11Y–5Gd–2Zn–0.5Zr (wt%). J Mater Sci 47:6263–6275. doi:10.1007/s10853-012-6546-4

    Article  Google Scholar 

  18. Yin DD, Wang QD, Boehlert CJ, Janik V, Gao Y, Ding WJ (2012) Creep behavior of Mg–11Y–5Gd–2Zn–0.5Zr (wt%) at 573 K. Mater Sci Eng A 546:239–247

    Article  Google Scholar 

  19. Yin DD, Wang QD, Gao Y, Chen CJ, Zheng J (2011) Effects of heat treatments on microstructure and mechanical properties of Mg–11Y–5Gd–2Zn–0.5Zr (wt%) alloy. J Alloy Compd 509:1696–1704

    Article  Google Scholar 

  20. Mordike BL, Stulíková I, Smola B (2005) Mechanisms of creep deformation in Mg-Sc-based alloys. Metall Mater Trans A 36:1729–1736

    Article  Google Scholar 

  21. Henry SD, Sanders BR, Hrivnak N (1993) ASM specialty handbook: aluminum and aluminum alloys. p 41

  22. Evangelista E, Spigarelli S (2002) Constitutive equations for creep and plasticity of aluminum alloys produced by powder metallurgy and aluminum-based metal matrix composites. Metall Mater Trans A 33:373–381

    Article  Google Scholar 

  23. Mirzadeh (2014) Constitutive analysis of Mg–Al–Zn magnesium alloys during hot deformation. Mech Mater 77:80

    Article  Google Scholar 

  24. Galiyev A, Kaibyshev R, Gottstein G (2001) Correlation of plastic deformation and dynamic recrystallization in magnesium alloy ZK60. Acta Mater 49:1199

    Article  Google Scholar 

  25. Yi SB, Zaefferer S, Brokmeier HG (2006) Mechanical behaviour and microstructural evolution of magnesium alloy AZ31 in tension at different temperatures. Mater Sci Eng A 424:275

    Article  Google Scholar 

  26. Jain J, Poole WJ, Sinclair CW, Gharghouri MA (2010) Reducing the tension–compression yield asymmetry in a Mg–8Al–0.5Zn alloy via precipitation. Scr Mater 62:301–304

    Article  Google Scholar 

  27. Hidalgo-Manrique P, Herrera-Solaz V, Segurado J, Llorca J, Gálvez F, Ruano OA, Yi SB, Pérez-Prado MT (2015) Origin of the reversed yield asymmetry in Mg-rare earth alloys at high temperature. Acta Mater 92:265–277

    Article  Google Scholar 

  28. Wang H, Boehlert CJ, Wang QD, Yin DD, Ding WJ (2016) Analysis of slip activity and deformation modes in tension and tension-creep tests of cast Mg–10Gd–3Y–0.5Zr (wt%) at elevated temperatures using in situ sem experiments. Metall Mater Trans A 47A:2421–2443

    Google Scholar 

  29. Liu K, Dong XH, Xie HY, Wu YJ, Peng F, Chen F (2016) Asymmetry in the hot deformation behavior of AZ31B magnesium sheets. Mater Sci Eng A 659:198–206

    Article  Google Scholar 

  30. Friedrich HE, Mordike BL (2006) Magnesium technology. Springer, Berlin, p 677

    Google Scholar 

  31. Christian JW, Mahajan S (1995) Deformation twinning. Prog Mater Sci 39:1

    Article  Google Scholar 

  32. Agnew SR, Duygulu Ö (2005) Plastic anisotropy and the role of non-basal slip in magnesium alloy AZ31B. Int J Plast 21:1161–1193

    Article  Google Scholar 

  33. Sarebanzadeh M, Mahmudi R, Roumina R (2015) Constitutive analysis and processing map of an extruded Mg–3Gd–1Zn alloy under hot shear deformation. Mater Sci Eng A 637:155–161

    Article  Google Scholar 

  34. Kula A, Noble K, Mishra RK, Niewczas M (2016) Plasticity of Mg–Gd alloys between 4 and 298 K. Philos Mag 96:134

    Article  Google Scholar 

  35. ChenYJ Wang QD, Peng JG, Zhai CQ (2006) Improving the mechanical properties of AZ31 Mg alloy by high ratio extrusion. Mater Sci Forum 503:865–870

    Article  Google Scholar 

  36. Wang H, Wang QD, Boehlert CJ, Yin DD, Yuan J (2015) Tensile and compressive creep behavior of extruded Mg–10Gd–3Y–0.5Zr (wt%) alloy. Mater Charact 99:25–37

    Article  Google Scholar 

  37. Barnett MR, Keshavarz Z, Beer AG, Atwell D (2004) Influence of grain size on the compressive deformation of wrought Mg–3Al–1Zn. Acta Mater 52:5093–5103

    Article  Google Scholar 

  38. Zhu SM, Nie JF, Mordike BL (2006) Creep and rupture properties of a squeeze-cast Mg-Al-Ca alloy. Metall and Mater Trans A 37:1221–1229

    Article  Google Scholar 

  39. Jansen AM, Dunand DC (1997) Creep of metals containing high volume fractions of unshearable dispersoids—Part II. Experiments in the Al-Al2O3 system and comparison to models. Acta Mater 45:4583–4592

    Article  Google Scholar 

  40. Dieter GE (1986) Mechanical metallurgy. McGraw-Hill, New York

    Google Scholar 

  41. Parkhomenko TA, Parkhomenko TA (1982) The low-temperature yield stress anomaly in metals and alloys. Physica Status Solidi (a) 7:11–42

    Article  Google Scholar 

  42. Suzuki T, Oya Y, Wee D (1980) Transition from positive to negative temperature dependence of the strength in Ni3–Ge–Fe3–Ge solid solution. Acta Metall 28(3):301–310

    Article  Google Scholar 

  43. Smola B, Stul Ková I, von Buch F, Mordike BL (2002) Structural aspects of high performance Mg alloys design. Mater Sci Eng A 324:113–117

    Article  Google Scholar 

  44. Chen XJ, Liu WC, Wu GH, Li YL, Li ZQ, Zhang S, Ding WJ (2016) High-temperature tensile and compressive behavior of peak-aged sand-cast Mg-10Gd-3Y-0.5Zr alloy. Adv Eng Mater 18:671–677

    Article  Google Scholar 

  45. Park SH, Lee JH, Moon BG, You BS (2014) Tension–compression yield asymmetry in as-cast magnesium alloy. J Alloy Compd 617:277–280

    Article  Google Scholar 

  46. Lou XY, Li M, Boger RK, Agnew SR, Wagoner RH (2007) Hardening evolution of AZ31B Mg sheet. Int J Plast 23:44–86

    Article  Google Scholar 

Download references

Funding

This study was supported by National Natural Science Foundation of China (No. 51401172), Project of Science & Technology Department of Sichuan Province (No. 2015HH0012), Fundamental Research Funds for the Central Universities (No. 2682014BR002), 2015 Cultivation Program for the Excellent Doctoral Dissertation of Southwest Jiaotong University, and the program of the 2015 Doctoral Innovation Founds of Southwest Jiaotong University.

Author information

Authors and Affiliations

Authors

Corresponding author

Correspondence to D. D. Yin.

Ethics declarations

Conflict of interest

The authors declare that they have no conflict of interest.

Rights and permissions

Reprints and permissions

About this article

Check for updates. Verify currency and authenticity via CrossMark

Cite this article

Lu, J.W., Yin, D.D., Ren, L.B. et al. Tensile and compressive deformation behavior of peak-aged cast Mg–11Y–5Gd–2Zn–0.5Zr (wt%) alloy at elevated temperatures. J Mater Sci 51, 10464–10477 (2016). https://doi.org/10.1007/s10853-016-0266-0

Download citation

  • Received:

  • Accepted:

  • Published:

  • Issue Date:

  • DOI: https://doi.org/10.1007/s10853-016-0266-0

Keywords

Navigation