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Preparation of meixnerite (Mg–Al–OH) type layered double hydroxide by a mechanochemical route

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Abstract

We have attempted to synthesize the meixnerite (Mg–Al–OH) type layered double hydroxide (LDH) by a two step milling operation of a mixture of Mg(OH)2 and Al(OH)3 with water. In the first-step, a mixture of the starting materials was milled for 1 h without water, and the product prepared in the first-step was milled for 2 h with water in the second-step milling operation. The milled products were characterized by X-ray diffraction (XRD), Fourier transform infrared (FTIR), and thermo gravimetric-differential thermal analyses with mass spectroscopy (TG-DTA/MS). The surface morphology was characterized by scanning electron microscopy (SEM). Meixnerite with a small amount of carbonate was successfully synthesized mechanochemically at ambient conditions by milling for only 3 h in a planetary ball mill.

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References

  1. Cavani F, Trifirò F, Vaccari A (1991) Catal Today 11:173

    Article  CAS  Google Scholar 

  2. Evans DG, Slade RCT (2006) In: Mingos DMP, Duan X, Evans DG (eds) Layered double hydroxides: structure and bonding, vol. 119. Springer-Verlag, Berlin, p 1

    Google Scholar 

  3. Li F, Duan X (2006) In: Mingos DMP, Duan X, Evans DG (eds) Layered double hydroxides: structure and bonding, vol 119. Springer-Verlag, Berlin, p 193

    Chapter  Google Scholar 

  4. Ulibarri MA, Hermosin MC, Basile F, Vaccari A, Monzón A, Romeo E, Marchi AJ, Costantino U, Nocchetti M, Hansen HCB (2001) In: Rives V (ed) Layered double hydroxides—present and future. Nova Science Publishers Inc, New York, p 251

    Google Scholar 

  5. Yamamoto T, Kodama T, Hasegawa N, Tsuji M, Tamaura Y (1995) Energy Convers Manage 36:637

    Article  CAS  Google Scholar 

  6. He J, Wei M, Li B, Kang Y, Evans DG, Duan X (2006) In: Mingos DMP, Duan X, Evans DG (eds) Layered double hydroxides: structure and bonding, vol 119. Springer-Verlag, Berlin, p 89

    Chapter  Google Scholar 

  7. de Roy A, Forano C, Besse JP (2001) In: Rives V (ed) Layered double hydroxides—present and future. Nova Science Publishers Inc, New York, p 1

    Google Scholar 

  8. Orinetto F, Ghiotti G, Graffin P, Tichit D (2000) Microporous Mesoporous Mater 39:229

    Article  Google Scholar 

  9. Oh JM, Hwang SH, Choy JH (2002) Solid State Ionics 151:285

    Article  CAS  Google Scholar 

  10. Mohan MR, Ramachandra BR, Jayalakshmi M, Swarna VJ, Srindhar B (2005) Mater Res Bull 40:347

    Article  Google Scholar 

  11. Lei X, Yang L, Zhang F, Duan X (2006) Chem Eng Sci 61:2730

    Article  CAS  Google Scholar 

  12. Rivera JA, Fetter G, Bosh P (2006) Microporous Mesoporous Mater 89:306

    Article  CAS  Google Scholar 

  13. Yun SK, Constantino VRL, Pinnavaia TJ (1995) Microporous Mater 4:21

    Article  CAS  Google Scholar 

  14. Sato T, Kato K, Endo T, Shimada M (1986) React Solids 2:253

    Article  CAS  Google Scholar 

  15. Gardner EA, Yun SK, Kwon T, Pinnavaia TJ (1998) Appl Clay Sci 13:479

    Article  CAS  Google Scholar 

  16. Tichit D, Bennani MN, Figueras F, Tessier R, Kervennal J (1998) Appl Clay Sci 13:401

    Article  CAS  Google Scholar 

  17. Tsyganok AI, Inaba M, Tsunoda T, Hamakawa S, Suzuki K, Hayakawa T (2003) Catal Commun 4:493

    Article  CAS  Google Scholar 

  18. Greenwell HC, Holliman PJ, Jones W, Velasco BV (2006) Catal Today 114:397

    Article  CAS  Google Scholar 

  19. Drits VA, Bookin AS (2001) In: Rives V (ed) Layered double hydroxides—present and future. Nova Science Publishers Inc, New York, p 39

    Google Scholar 

  20. Rives V (2001) In: Rives V (ed) Layered double hydroxides—present and future. Nova Science Publishers Inc, New York, p 115

    Google Scholar 

  21. Lopez T, Bosch P, Asomoza M, Gomez R, Ramos E (1997) Mater Lett 31:311

    Article  CAS  Google Scholar 

  22. Xie X, An X, Wang X, Wang Z (2003) J Nat Gas Chem 12:259

    CAS  Google Scholar 

  23. Zhang J, Zhang F, Ren L, Evans DG, Duan X (2004) Mater Chem Phys 85:207

    Article  CAS  Google Scholar 

  24. Othman MR, Rasid NM, Fernado WJN (2006) Chem Eng Sci 61:1555

    Article  CAS  Google Scholar 

  25. Kloprogge JT, Frost RL (2001) In: Rives V (ed) Layered double hydroxides—present and future. Nova Science Publishers Inc, New York, p 139

    Google Scholar 

  26. Kloprogge JT, Wharton D, Hickey L, Frost RL (2002) Am Mineral 87:623

    Article  CAS  Google Scholar 

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Authors and Affiliations

  1. Institute of Multidisciplinary Research for Advanced Materials, Tohoku University, 2-1-1, Katahira, Aoba-Ku, Sendai, 980-8577, Japan

    William Tongamp, Qiwu Zhang & Fumio Saito

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  1. William Tongamp
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  2. Qiwu Zhang
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  3. Fumio Saito
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Correspondence to Qiwu Zhang.

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Tongamp, W., Zhang, Q. & Saito, F. Preparation of meixnerite (Mg–Al–OH) type layered double hydroxide by a mechanochemical route. J Mater Sci 42, 9210–9215 (2007). https://doi.org/10.1007/s10853-007-1866-5

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  • DOI: https://doi.org/10.1007/s10853-007-1866-5

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