Abstract
Composite WO3–Nb2O5 thin films were deposited on the glass and fluorine-doped tin oxide (FTO)-coated glass substrates using simple and inexpensive spray pyrolysis technique. The process parameters, like nozzle-to-substrate distance, spray rate, concentration of sprayed solution, etc., were optimized to good quality films. The films were characterized for the structural, morphological, optical, and electrochromic properties. Structural and morphological characterizations of the films were carried out using scanning electron microscopy and X-ray diffraction techniques. Electrochemical properties of the Composite WO3–Nb2O5 thin films were further studied using cyclic-voltammetry, chronoamperometry, chronocoulometry, and electrochemical Impedance spectroscopy.
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Mujawar SH, Inamdar AI, Patil SB, Patil PS (2006) Solid State Ionics 177:3333
Mujawar SH, Inamdar AI, Betty CA, Ganesan V, Patil PS (2007) Electrochim Acta 52:4899
Granqvist CG (1995) Handbook of inorganic electrochromic materials. Elsevier Publication, Amsterdam
Monk PMS, Mortimer RJ, Rosseinsky DR (1995) Electrochromism fundamental and applications. VCH, Weinheim
Hashimoto S, Matsuoka H (1991) J Electrochem Soc 138:2403
Pennisi A, Simone F, Lampert CM (1992) Sol Energy Mater Sol Cells 28:223
Rougier A, Blyr A, Quede A (2001) J Electrochem Soc 148(2):H7
Ozer N, Lampert CM (1999) Thin Solid Films 349:205
Richardson TJ, Von Rottkay K, Slack J, Michalak F, Rubin M (1998) Electrochem Soc Proc 98–26 158
Schmitt M, Aegerter MA (2001) Electrochim Acta 46:2105
Rosario AV, Pereira EC (2001) Electrochim Acta 46:1905
Costa ED, Avellaneda CO, Pawlicka A (2001) J Mater Sci 36:1407
Pehlivan E, Tepehan FZ, Tepehan GG (2005) Sol Energy Mater Sol Cells 87:317–322
Pehlivan E, Tepehan FZ, Tepehan GG (2003) Solid State Ionics 165:105–110
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Authors are very much thankful to the CSIR, New Delhi for the financial support extended through Senior Research Fellowship (SRF).
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Mujawar, S.H., Inamdar, A.I., Betty, C.A. et al. Electrochromism in composite WO3–Nb2O5 thin films synthesized by spray pyrolysis technique. J Appl Electrochem 41, 397–403 (2011). https://doi.org/10.1007/s10800-010-0249-9
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DOI: https://doi.org/10.1007/s10800-010-0249-9