Skip to main content
SpringerLink
Log in

Phases Obtained by Mechanoactivation in Ceramic Based on Calcium Phosphate Nanopowders with Ca/P = 1.25

  • BIOMATERIALS
  • Published:
Glass and Ceramics Aims and scope Submit manuscript

The processes occurring during the mechanoactivation of powders and firing of samples pressed from calcium phosphate nanopowders with molar ratio Ca/P = 1.25 were studied. As a result of washing nanopowder in distilled water and alcohol after mechanoactivation ammonium phosphates were removed and only hydroxyapatite and tricalcium phosphate were present in the ceramic. To preserve the molar ratio Ca/P = 1.25 in the ceramic washing should not be performed, and then after firing, aside from the indicated phases, calcium pyrophosphate is also present in the ceramic.

This is a preview of subscription content, log in via an institution to check access.

Access this article

Log in via an institution

Price excludes VAT (USA)
Tax calculation will be finalised during checkout.

Instant access to the full article PDF.

Institutional subscriptions

Fig. 1.
Fig. 2.
Fig. 3.
Fig. 4.

Similar content being viewed by others

References

  1. A. G. Veresov, V. I. Putlyaev, and Yu. D. Tret’yakov, “Advancements in the field of calcium phosphate biomaterials,” Ross. Khim. Zh., 44(6) (Pt. 2), 32 – 46 (2000).

    Google Scholar 

  2. S. M. Barinov and V. S. Komlev, Bioceramic based on Calcium Phosphates [in Russian], Nauka, Moscow (2005).

    Google Scholar 

  3. Material Used in Endoprostheses [Electronic resource]; URL: http://www.medintention.ru/ joms-816-1.html.

  4. T. V. Safronova, V. I. Putlyaev,M. A. Shekhirev, and Yu. D. Tret’yakov, “Method of obtaining ceramic biodegradable material consisting of calcium pyrophosphate and tricalcium phosphate, RF Patent 2391316, No. 2008152281/03,” Byull. Izobr. Polezn. Modeli, No. 16 (2010); December 30, 2008; published June 10, 2010.

  5. M. N. Safina, T. V. Safronova, and E. S. Lukin, “Calcium phosphate based ceramic with a resorbable phase and low sintering temperature,” Steklo Keram., No. 8, 19 – 24 (2007); M. N. Safina, T. V. Safronova, and E. S. Lukin, “Calcium phosphate based ceramic with a resorbable phase and low sintering temperature,” Glass Ceram., 64(7 – 8), 238 – 243 (2007).

  6. A. V. Belyakov, E. S. Lukin, T. V. Safronova, M. N. Safina, and V. I. Putlyaev, “Porous materials made from calcium phosphates (Review),” Steklo Keram., No. 10, 17 – 19 (2008); A. V. Belyakov, E. S. Lukin, T. V. Safronova, M. N. Safina, and V. I. Putlyaev, “Porous materials made from calcium phosphates (Review),” Glass Ceram., 65(9 – 10), 337 – 339 (2008).

  7. F. H. Albee and H. F. Morrison, “Studies in bone growth – triple calcium phosphate as a stimulus to osteogenesis,” Ann. Surg., 7, 32 – 39 (1920).

    Google Scholar 

  8. A. S. Vlasov and T. A. Karabanova, “Ceramics and medicine (review),” Steklo Keram., No. 9 – 10, 23 – 25 (1993); A. S. Vlasov and T. A. Karabanova, “Ceramics and medicine (review),” Glass Ceram., 50(9 – 10), 398 – 401 (1993).

  9. N. V. Petrakova, Effect of Synthesis and Sintering Conditions for Nanopowders of Hydroxyapatite on the Formation of the Microstructure and Properties of Ceramic, Author’s Abstract of Candidate’s Thesis [in Russian], May 17, 2011, Moscow (2014).

  10. J. C. Elliot, Structure and Chemistry of the Apatites and Other Calcium Orthophosphates, Elsevier, Amsterdam (1994).

    Google Scholar 

  11. T. V. Safronova, “Phase composition of ceramic based on calcium hydroxyapatite powders containing byproducts of the synthesis reaction,” Steklo Keram., No. 4, 21 – 24 (2009); T. V. Safronova, “Phase composition of ceramic based on calcium hydroxyapatite powders containing byproducts of the synthesis reaction,” Glass Ceram., 66(3 – 4), 136 – 139 (2009).

  12. A. I. Volkov and I. M. Zharskii, Great Chemical Handbook [in Russian], Sovremennaya shkola, Moscow (2005).

    Google Scholar 

  13. A. I. Efimov, I. P. Belorukova, I. V. Vasil’kova, et al., Handbook of the Properties of Inorganic Compounds [in Russian], Khimiya, Leningrad (1983).

    Google Scholar 

  14. V. V. Boldyrev, “Mechanochemistry and the mechanical activation of solid substances,” Usp. khim., 75(3), 203 – 216 (2006).

    Article  Google Scholar 

  15. V. S. Bakunov, et al., A. V. Belyakov, N. T. Dzhigailo, and R. Ya. Popil’skii, “On the possibility of obtaining dense ceramic from zirconates of alkaline-earth metals during combined synthesis and sintering,” Tr. MKhTI im. D. I. Mendeleeva, No. 128, 67 – 71 (1983).

Download references

Author information

Authors and Affiliations

  1. D. I. Mendeleev Russian University of Chemical Technology, Moscow, Russia

    N. V. Gudimov & A. V. Belyakov

Authors
  1. N. V. Gudimov
    View author publications

    You can also search for this author in PubMed Google Scholar

  2. A. V. Belyakov
    View author publications

    You can also search for this author in PubMed Google Scholar

Corresponding author

Correspondence to A. V. Belyakov.

Additional information

Translated from Steklo i Keramika, No. 12, pp. 42 – 46, December, 2017.

Rights and permissions

Reprints and permissions

About this article

Check for updates. Verify currency and authenticity via CrossMark

Cite this article

Gudimov, N.V., Belyakov, A.V. Phases Obtained by Mechanoactivation in Ceramic Based on Calcium Phosphate Nanopowders with Ca/P = 1.25. Glass Ceram 74, 460–463 (2018). https://doi.org/10.1007/s10717-018-0016-7

Download citation

  • Published:

  • Issue Date:

  • DOI: https://doi.org/10.1007/s10717-018-0016-7

Key words

Search

Navigation