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Synthesis of pyrido[3',2':4,5]thieno[3,2-d]-[1,3,2]diazaphosphorine derivatives

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Chemistry of Heterocyclic Compounds Aims and scope

Refluxing 3-aminothieno[2,3-b]pyridine-2-carboxamides with P4S10 in dry pyridine gave the substituted 2-mercapto-2,3-dihydropyrido[3',2':4,5]thieno[3,2-d][1,3,2]diazaphosphorin-4(1H)-one-2-thiones and/or -2,4(1H)-dithiones as 1:1 complexes with pyridine.

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Authors and Affiliations

  1. “ChemEx” Laboratory, Vladimir Dal’ East Ukrainian National University, 20-A/7 Molodyozhnyi Kv, Lugansk, 91034, Ukraine

    V. V. Dotsenko & S. G. Krivokolysko

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  1. V. V. Dotsenko
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  2. S. G. Krivokolysko
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Correspondence to V. V. Dotsenko.

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Translated from Khimiya Geterotsiklicheskikh Soedinenii, No. 12, pp. 1987-1991, December, 2012.

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Dotsenko, V.V., Krivokolysko, S.G. Synthesis of pyrido[3',2':4,5]thieno[3,2-d]-[1,3,2]diazaphosphorine derivatives. Chem Heterocycl Comp 48, 1863–1867 (2013). https://doi.org/10.1007/s10593-013-1220-6

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  • DOI: https://doi.org/10.1007/s10593-013-1220-6

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