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Synthesis of n-methyl-3-carboxy-2-chloro-dibenzo[c,f][1,4,5]oxa-thiazepine s,s-dioxide and its derivatives

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Chemistry of Heterocyclic Compounds Aims and scope

A new dibenzo-condensed oxathiazepinecarboxylic acid was obtained starting from the methyl ester of 2,4-dichloro-5-chlorosulfonylbenzoic acid. Derivatives were obtained from N-phenylamide and N-methylamide of 2,4-dichloro-5-chlorosulfonylbenzoic acid. Methods for the preparation of the starting aromatic sulfonyl chlorides were proposed.

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Correspondence to A. S. Bychenkov.

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Translated from Khimiya Geterotsiklicheskikh Soedinenii, No. 11, pp. 1728–1733, November, 2009.

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Bychenkov, A.S., Tarasov, A.V., Pisarev, P.K. et al. Synthesis of n-methyl-3-carboxy-2-chloro-dibenzo[c,f][1,4,5]oxa-thiazepine s,s-dioxide and its derivatives. Chem Heterocycl Comp 45, 1391–1395 (2009). https://doi.org/10.1007/s10593-010-0438-9

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  • DOI: https://doi.org/10.1007/s10593-010-0438-9

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