Advertisement

Chemistry of Heterocyclic Compounds

, Volume 43, Issue 4, pp 434–438 | Cite as

Synthesis of 3-N-substituted exo-3,4 diazatricyclo[5.2.1.02,6]dec-4-enes

  • E. A. Shafikova
  • D. V. Petrov
  • V. A. Dokichev
Article
  • 46 Downloads

Abstract

Treatment of exo-3,4-diazatricyclo[5.2.1.02,6]dec-4-ene with methyl acrylate, acrylonitrile, ethylene oxide, acetic acid and nitrosonium cation gave a series of 3-N-substituted exo-3,4-diazatricyclo[5.2.1.02,6]dec-4-enes.

Keywords

pyrazolines exo-3,4-diazatricyclo[5.2.1.02,6]dec-4-ene alkylation acylation nitrosation 

Preview

Unable to display preview. Download preview PDF.

Unable to display preview. Download preview PDF.

References

  1. 1.
    Yu. V. Tomilov, I. V. Kostyuchenko, and O. M. Nefedov, Usp. Khim., 69, 507 (2000).Google Scholar
  2. 2.
    H. Krieger, Arzneim.-Forsch., 18, 129 (1968).Google Scholar
  3. 3.
    H. Krieger, Arzneim.-Forsch., 18, 324 (1968).Google Scholar
  4. 4.
    H. Krieger, Arzneim.-Forsch., 18, 487 (1968).Google Scholar
  5. 5.
    E. A. Yatsynich, D. V. Petrov, V. A. Dokichev, and Yu. V. Tomilov, Zh. Org. Khim., 41, 1187 (2005).Google Scholar
  6. 6.
    D. V. Petrov, V. A. Gorpinchenko, E. A. Shafikov, F. S. Zarudnii, N. Zh. Baschenko, R. Yu. Khisamutdinova, N. S. Makara, V. A. Vakhitov, Yu. V. Vakhitova, Chzhan Veimu, R. I. Alimbekov, V. A. Dokichev, Yu. V. Tomilov, and O. M. Nefedov, Russian Patent 2281939; Byul. Izobr., No. 23 (2006).Google Scholar
  7. 7.
    V. A. Gorpinchenko, E. A. Yatsynich, D. V. Petrov, L. T. Karachurina, R. Yu. Khisamutdinova, N. Zh. Baschenko, V. A. Dokichev, Yu. V. Tomilov, M. S. Yunusov, and O. M. Nefedov, Khim.-Farm. Zh., 39, No. 6, 9 (2005).Google Scholar
  8. 8.
    A. Esanu, Belg. Patent 902231; Chem. Abstr., 104, 110121 (1985).Google Scholar
  9. 9.
    A. V. Stepakov, A. P. Molchanov, and R. R. Kostikov, Zh. Org. Khim., 41, 252 (2005).Google Scholar
  10. 10.
    A. N. Kost, G. V. Golubeva, and R. G. Stepanov, Zh. Org. Khim., 32, 2240 (1962).Google Scholar
  11. 11.
    A. P. Molchanov, A. V. Stepakov, and R. R. Kostikov, Zh. Org. Khim., 40, 1561 (2004).Google Scholar
  12. 12.
    A. P. Molchanov, A. V. Stepakov, V. M. Boitsov, Yu. Kopf, and R. R. Kostikov, Zh. Org. Khim., 39, 118 (2003).Google Scholar
  13. 13.
    A. P. Molchanov, A. V. Stepakov, V. M. Boitsov, and R. R. Kostikov, Zh. Org. Khim., 38, 1723 (2002).Google Scholar
  14. 14.
    G. C. Levy and G. L. Nelson, Carbon-13 Nuclear Magnetic Resonance for Organic Chemists [Russian translation], Mir., Moscow (1975), p. 71.Google Scholar

Copyright information

© Springer Science+Business Media, Inc. 2007

Authors and Affiliations

  • E. A. Shafikova
    • 1
  • D. V. Petrov
    • 1
  • V. A. Dokichev
    • 1
  1. 1.Institute of Organic Chemistry, Ufa Science CenterRussian Academy of SciencesUfa

Personalised recommendations