Abstract
A simple method for the synthesis of 1,2-ditellurolane is proposed, based on the reaction of elemental tellurium with 1,3-dihalopropane in a system of hydrazine hydrate and alkali followed by the effect of organic solvent on the first formed poly(trimethyleneditellurides). The products of the oxidation and reduction of 1,2-ditellurolane were characterized and its spectral characteristics were analyzed.
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Dedicated To Academician Of The Russian Academy Of Science Mikhail Grigor’evich Voronkov on his 85th Birthday.
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Translated from Khimiya Geterotsiklicheskikh Soedinenii, No. 11, 1705–1713, November 2006.
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Russavskaya, N.V., Elaev, A.V., Grabel’nyh, V.A. et al. 1,2-Ditellurolane: A new synthetic method, structure and chemical reactions. Chem Heterocycl Compd 42, 1464–1471 (2006). https://doi.org/10.1007/s10593-006-0263-3
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DOI: https://doi.org/10.1007/s10593-006-0263-3