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Chemistry of Heterocyclic Compounds

, Volume 42, Issue 7, pp 907–913 | Cite as

Molecular and crystal structure of 1,2-dihydro-3H-1,3,4-benzotriazepines

  • Yu. M. Chumakov
  • Yu. A. Simonov
  • G. Bocelli
  • M. Gdaniec
  • S. V. Vlassiuk
  • V. I. Pavlovsky
Article

Abstract

Three novel 1,2-dihydro-3H-1,3,4-benzotriazepines have been synthesized: 7-bromo-5-phenyl-3-phenylcarbamoyl-1,2-dihydro-3H-1,3,4-benzotriazepin-2-one, 7-bromo-5-phenyl-1,2-dihydro-3H-1,3,4-benzotriazepin-2-thione, and 7-methyl-5-phenyl-1,2-dihydro-3H-1,3,4-benzotriazepin-2-one. Their crystal structures have been determined using X-ray analysis.

Keywords

benzotriazepine hydrogen bonds crystal structure X-ray analysis 

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Copyright information

© Springer Science+Business Media, Inc. 2006

Authors and Affiliations

  • Yu. M. Chumakov
    • 1
  • Yu. A. Simonov
    • 1
  • G. Bocelli
    • 2
  • M. Gdaniec
    • 3
  • S. V. Vlassiuk
    • 4
  • V. I. Pavlovsky
    • 4
  1. 1.Institute of Applied Physics of Academy of Sciences of MoldovaKishinevMoldavian Republic
  2. 2.IMEM-CNRParmaItaly
  3. 3.Chemistry FacultyA. Mickiewicz UniversityPoznanPoland
  4. 4.A. V. Bogatsky Physico-Chemical InstituteUkraine National Academy of SciencesOdessa

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