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Extraction and pre-concentration of ketamine by using a three-dimensional spongin-based scaffold of the Haliclona sp. marine demosponge origin

  • T.C. Biological and Biomimetic Materials
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Abstract

In this research, a novel renewable biomaterial spongin of marine sponge origin has been used as adsorbent in a miniaturized method based on solid-phase extraction (SPE) for the pre-concentration and determination of ketamine. The subsequent determinations of ketamine have been performed by high-performance liquid chromatography. Various potential effective factors during extraction procedure including pH value, amount of adsorbent, elution volume and its type, washing volume and its ratio, extraction time and salt concentration of the sample solution were optimized. Under the optimized conditions, the linear dynamic range for ketamine determination was 10–1000 ng mL−1. The relative standard deviation (RSD%, n = 5) for determination of ketamine (20 ng mL−1) was 2.8%, and the calculated limit of detection was 1.7 ng mL−1. The developed SPE procedure has been successfully applied for analysis of ketamine in water, urine and apple juice samples with high precision and accuracy.

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Authors and Affiliations

  1. Department of Chemistry, Faculty of Basic Sciences, Imam Hossein University, Tehran, Iran

    Vahid Ashouri & Kourosh Adib

  2. Chemical Injuries Research Center, Systems Biology and Poisonings Institute, Baqiyatallah University of Medical Sciences, Tehran, Iran

    Mehdi Rahimi-Nasrabadi

  3. Faculty of Pharmacy, Baqiyatallah University of Medical Sciences, Tehran, Iran

    Mehdi Rahimi-Nasrabadi

  4. Department of Marine Biology, Faculty of Marine Sciences, Chabahar Maritime University, Daneshgah Ave., 99717-56499, Chabahar, Iran

    Gilan Attaran Fariman

  5. Department of Marine Chemistry, Faculty of Marine Sciences, Chabahar Maritime University, Chabahar, Iran

    Vahid Ashouri & Mir Mahdi Zahedi

  6. Center of Excellence in Electrochemistry, School of Chemistry, College of Science, University of Tehran, Tehran, Iran

    Mohammad Reza Ganjali

  7. Biosensor Research Center, Endocrinology and Metabolism Molecular Cellular Sciences Institute, Tehran University of Medical Sciences, Tehran, Iran

    Mohammad Reza Ganjali

  8. Faculty of Pharmacy, Tabriz University of Medical Sciences, Tabriz, Iran

    Elnaz Marzi Khosrowshahi

Authors
  1. Vahid Ashouri
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  2. Mehdi Rahimi-Nasrabadi
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  3. Gilan Attaran Fariman
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  4. Kourosh Adib
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  5. Mir Mahdi Zahedi
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  6. Mohammad Reza Ganjali
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  7. Elnaz Marzi Khosrowshahi
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Correspondence to Mehdi Rahimi-Nasrabadi.

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Ashouri, V., Rahimi-Nasrabadi, M., Attaran Fariman, G. et al. Extraction and pre-concentration of ketamine by using a three-dimensional spongin-based scaffold of the Haliclona sp. marine demosponge origin. Appl. Phys. A 126, 421 (2020). https://doi.org/10.1007/s00339-020-03598-z

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  • DOI: https://doi.org/10.1007/s00339-020-03598-z

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