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Macroheterocycles. 5. Synthesis of macrocyclic amido esters and amido thioesters on the basis of derivatives of α-hydroxy and α-mercapto acids

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Chemistry of Heterocyclic Compounds Aims and scope

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Abstract

3,6-Dioxa-4-keto-, 2-benzyl-3,6-dioxa-4-keto-, and 3-oxa-6-thio-5-ketooctanedioic acids were obtained by the reaction of diglycolic acid anhydride with glycolic, β-phenyllactic, and thioglycolic acids. 2,9-Dibenzyl-3,8-dioxa-4,7-diketodecanoic acid was obtained by the reaction of succinyl chloride with β-phenyllactic acid. Eight macrocyclic amido esters and amido thioesters that are new polydentate macrocyclic ligands were synthesized by the reaction of the chlorides of the acids obtained with 3-oxa-1,5-diaminopentane, 3,6-dioxa-1,8-diaminooctane, and 1,4-diaminobutane.

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Literature cited

  1. A. V. Bogat-skii, N. G. Luk'yanenko, V. A. Shapkin, M. S. Salakhov, M. U. Mamina, and D. Taubert, Zh. Org. Khim.,16 (1980, in press).

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Authors and Affiliations

  1. Physicochemical Institute, Academy of Sciences of the Ukrainian SSR, 270080, Odessa

    N. G. Luk'yanenko, A. V. Bogat-skii & Yu. A. Popkov

Authors
  1. N. G. Luk'yanenko
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  2. A. V. Bogat-skii
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  3. Yu. A. Popkov
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Additional information

See [1] for communication 4.

Translated from Khimiya Geterotsiklicheskikh Soedinenii, No. 3, pp. 306–309, March, 1980.

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Luk'yanenko, N.G., Bogat-skii, A.V. & Popkov, Y.A. Macroheterocycles. 5. Synthesis of macrocyclic amido esters and amido thioesters on the basis of derivatives of α-hydroxy and α-mercapto acids. Chem Heterocycl Compd 16, 222–225 (1980). https://doi.org/10.1007/BF02401712

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  • DOI: https://doi.org/10.1007/BF02401712

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