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Synthesis and NMR spectroscopic study of derivatives of pyrazolo[1,5-a]pyrimidines

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Chemistry of Heterocyclic Compounds Aims and scope

Abstract

Reactions of 3,5-diamino-4-nitropyrazole with asymmetric β-dicarbonyl compounds formed pyrazolo[1,5-a]pyrimidines, which in turn were used as the starting compounds in the reaction with dimethylformamide diethylacetal. The structure of the compounds obtained was studied by NMR spectroscopy in experiments involving the homonuclear Overhauser effect.

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References

  1. N. P. Solov'eva, V. A. Makarov, and V. G. Granik, Khim. Geterotsikl. Soedin., No. 1, 89 (1997).

    Google Scholar 

  2. V. A. Makarov, O. S. Anisimova, and V. G. Granik, Khim Geterotsikl. Soedin., No. 3, 329 (1997).

    Google Scholar 

  3. V. G. Granik, Usp. Khim.,53, No. 4, 651 (1984).

    Google Scholar 

  4. R. L. Reeves, The Chemistry of the Carbonyl Group, Patai. et al. (eds.), London-New York-Sydney-Toronto (1966), p. 610.

  5. V. G. Granik, A. M. Zhidkova, and R. G. Glushkov, Usp. Khim.,46, No. 4, 685 (1977).

    Google Scholar 

  6. A. Holy, S. Chladek, and J. Zemlitka, Coll. Czech. Chem. Commun.,34, 253 (1969).

    Google Scholar 

  7. F. W. Wehrli and T. Wirthlin, Interpretation of Carbon-13 NMR Spectra, Heyden and Son Ltd., London (1976).

    Google Scholar 

  8. V. G. Granik, A. M. Zhidkova, I. S. Zhivotovskaya, N. P. Solov'eva, and M. K. Polievktov, Zh. Org. Khim.,17, No. 11, 2421 (1981).

    Google Scholar 

  9. N. Takeuchi, N. Okada, and S. Tabinaga, Chem. Pharm. Bull.,31, 4355 (1983).

    Google Scholar 

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Authors
  1. V. A. Makarov
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  2. N. P. Solov'eva
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  3. V. G. Granik
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Additional information

Center for Chemistry of Medicinal Substances (TsKhLS-VNIKhFI), Moscow 119815. Translated from Khimiya Geterotsiklicheskikh Soedinenii, No. 5, pp. 619–628, May, 1997.

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Makarov, V.A., Solov'eva, N.P. & Granik, V.G. Synthesis and NMR spectroscopic study of derivatives of pyrazolo[1,5-a]pyrimidines. Chem Heterocycl Compd 33, 535–542 (1997). https://doi.org/10.1007/BF02291935

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  • DOI: https://doi.org/10.1007/BF02291935

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