Abstract
Derivatives of 2H-5,6-dihydro-1,3-thiazine are formed by the reaction of acetothioacetic acid ethyl ester with aromatic aldehydes on heating in ethanol in the presence of aqueous ammonia.
Similar content being viewed by others
References
B. A. Vigante, J. J. Ozols, G. J. Duburs, E. M. Belash, and J. I. Beilis,Khim. Geterotsikl. Soedin., No. 2, 210 (1984).
M. Barfield and B. Chakrabarti,Chem. Rev.,69, 757 (1969).
M. Thiel, F. Asinger, and G. Trümpler,Liebigs Ann. Chem.,619, 137 (1958).
F. Asinger, M. Thiel, and W. Höringklee,Liebigs Ann. Chem.,610, 1 (1948).
J. C. Getson, J. M. Greene, and A. I. Meyers,J. Heterocycl. Chem.,1, 300 (1964).
G. M. Sheldrick,Acta Crystallogr.,A46, 467 (1990).
G. M. Sheldrick, SHELXS-86. Program for the Solution of Crystal Structures, University of Göttingen (1985).
G. M. Sheldrick,SHELXL-93, Program for the Refinement of Crystal Structures, University of Göttingen (1993).
Additional information
Latvian Institute of Organic Chemistry, Riga LV-1006, Latvia; e-amil: arcady@osi.lv. Translated from Khimiya Geterotsiklicheskikh Soedinenii, No. 7, pp. 978–985, July, 2000.
Rights and permissions
About this article
Cite this article
Vigante, B., Ozols, J., Mishnev, A. et al. Formation of derivatives of 5,6-dihydro-1,3-thiazines in the reaction of acetothioacetic acid ethyl ester under the conditions of the Hantzsch synthesis. Chem Heterocycl Compd 36, 862–869 (2000). https://doi.org/10.1007/BF02256924
Received:
Issue Date:
DOI: https://doi.org/10.1007/BF02256924