Abstract
A method has been proposed for the synthesis of 2-trihalomethyl-1, 3,5-dithiazines based on the reaction of 1 1, -dithiols with 1, 1-dichloro- and I -chloroalkyl isocyanates. The thermal stability and mass spectra of these compounds were studied.
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References
I. V. Koval', Usp. Khim.,62, No. 4, 813 (1993).
C. Giordano and A. Belli, Synthesis, No. 3, 193 (1977).
V. I. Gorbatenko and L. 1. Samarai, Synthesis, No. 2, 85 (1980).
L. I. Samarai, V. I. Gorbatenko, and M. V. Vovk, Ukr. Khim. Zh.,55, 966 (1989).
L. I. Samarai, V. I. Boiko, and M. N. Gertsyuk, Zh. Org. Khim.,26, 475 (1990).
M. V. Vovk, V I. Dorokhov, and L. I. Samari, Ukr. Khim. Zh.,25, 2394 (1989).
V. V. Vovk, V. I. Boiko, and L. I. Samari, Ukr. Khim. Zh.,59, 1081 (1993).
M. V. Vovk, V. I. Dorokhov, V. I. Boiko, and L. I. Samarai, Khim. Geterotsikl. Soedin., No. 11, 1472 (1993).
J. Jentzsch, J. Fobian, and R. Mayer, Chem. Ber.,95, 1764 (1962).
M. N. Polmer, Org. Mass Spectrom.,5, 1085 (1971).
D. C. De Jongh and M. L. Thomson, J. Org. Chem.,38, 1356 (1973).
D. Schumann, E. Frese, and A. Schonberg, Chem. Ber.,102, 3192 (1969).
I. C. Calder, Org. Mass Spectrom.,3, 453 (1970).
P. H. Chen, J. Org. Chem.,41, 2973 (1976).
Additional information
Institute of Organic Chemistry, National Academy of Sciences of Ukraine, 252660 Kiev, Ukraine. Translated from Khimiya Geterotsiklicheskikh Soedinenii, No. 7, pp, 996–1000, July, 1995. Original article submitted February 21, 1995.
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Vovk, M.V., Krainikova, I.G. & Dorokhov, V.I. Synthesis, thermal stability and mass spectra of 2-trihalomethyl-1,3,5-dithiazin-4-ones and their 2,3-dihydro derivatives. Chem Heterocycl Compd 31, 868–872 (1995). https://doi.org/10.1007/BF01170751
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DOI: https://doi.org/10.1007/BF01170751