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Chemistry of Heterocyclic Compounds

, Volume 30, Issue 6, pp 696–700 | Cite as

Synthesis and spatial structure of methyl substituted 2-phenylpiperidine-4-spiro-5′-imidazolidine-2′,4′-diones

  • B. V. Unkovskii
  • M. Yu. D'yakov
  • G. V. Cherkaev
  • T. D. Sokolova
Article
  • 37 Downloads

Abstract

Piperidine-4-spiro-5′-irnidazolidine-2′, 4′-diones have been synthesized from the appropriate methyl substituted 2 phenyl-4-hydroxypiperidines and 4-cyano-4-aminopiperidines by the Bucherer—Bergs and Strecker methods. The stereocheinical composition and spatial structure of the compounds synthesized have been established from1H and13C NMR data.

Keywords

Methyl Organic Chemistry Spatial Structure Diones 
These keywords were added by machine and not by the authors. This process is experimental and the keywords may be updated as the learning algorithm improves.

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References

  1. 1.
    H. T. Bucherer and W. Steiner, J. Prakt. Chem.,140, 291 (1934).Google Scholar
  2. 2.
    H. T. Bucherer and V. A. Lieb, J. Prakt. Chem.,141, 5 (1934).Google Scholar
  3. 3.
    L. C. Avendono and G. G. Trigo, Adv. Heterocycl. Chem.,38, 177 (1985).Google Scholar
  4. 4.
    S. A. Avetisyan, L. V. Azaryan, and S. L. Kocharov, Arm. Khim. Zh.,39, 151 (1986).Google Scholar
  5. 5.
    J. T. Edward and C. Jitraugsri, Can. J. Chem.,53, 3339 (1975).Google Scholar
  6. 6.
    B. V. Unkovskii, M. Yu. D'yakov, T. D. Sokolova, G. V. Cherkaev, and V. B. Rozhnov, Khim. Geterotsiki. Soedin., No. 12, 1628 (1992).Google Scholar
  7. 7.
    N. M. Sergeev, NMR Spectroscopy [in Russian], Mosc. Unit, Moscow (1981), p. 279.Google Scholar
  8. 8.
    M. Yu. D'yakov, T. D. Sokolova, A. V. Peretokin, A. S. Moskovkin, and B. V. Unkovskii, Khim. Geterotsikl. Soedin., No. 2, 224 (1991).Google Scholar
  9. 9.
    B. V. Unkovskii, M. Yu. D'yakov, T. D. Sokolova, V. B. Rozhnov, and G. V. Cherkaev, Khim. Geterotsikl. Soedin., No. 12, 1621 (1992).Google Scholar

Copyright information

© Plenum Publishing Corporation 1995

Authors and Affiliations

  • B. V. Unkovskii
  • M. Yu. D'yakov
  • G. V. Cherkaev
  • T. D. Sokolova

There are no affiliations available

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