Abstract
2,2,3,3-Tetracyano-7,8-dithiabicyclo[3.2.1]octanes were formed in the reaction of dithiocarboxyclic acid allyl and cinnamyl esters with tetracyanoethylene, and their structure was determined by a number of physico-chemical methods, including x-ray structural study.
Similar content being viewed by others
References
I. V. Magedov, V. N. Drozd, S. Yu. Shapakin, D. S. Yufit, and Yu. T. Struchkov, Sulfur Lett., 17 (1994).
F. H. Allen, O. Kennard, D. G. Watson, L Brummer, A. G. Orpen and R. Taylor, J. Chem. Soc. Perkin II. No. 1, 1(1987).
H. Gotthardt, O. M. Huss, and S. Schog-Tribbensee, Chem. Ber.,114, 285 (1981).
B. Kojic-Prodic, Z. Ruzic-Toros, and J. J. Herak, Acta Crystallogr.,B37, 214 (1981).
I. R. Fjeldskaar, D. Grace, C. Romming, and L. Scattebol, Acta Chem. Scand.,B42, 280 (1988).
C. A. G. Haasnoot, F. A. A. M. de Leeuw, and C. Altona, Tetrahedron,36, 2783 (1900).
N. L. Allinger and J. T. Sprague, J. Am. Chem. Soc.,95, 3893 (1973).
J. Kao and N. L. Allinger, J. Am. Chem. Soc.,99, 975 (1977).
H. Günther, Introduction m NMR Spectroscopy [Russian translation], Mir, Moscow (1984), pp. 132, 404.
G. M. Sheldrick, SHELXTL PLUS. PC Version, Siemens Analytical X-ray Instruments, Inc., Madison, Wisconsin (1989).
Additional information
K. A. Timiryazev Agricultural Academy, Moscow 127550. A. N. Nesmeyanov Institute of Organometallic Compounds, Russian Academy of Sciences, Moscow 117813. Translated from Khimiya Geterotsiklicheskikh Soedinenii, No. 6, pp. 770–780. June, 1994. Original article submitted May 18, 1994. eskikh Soedinenii, No. 6, pp. 770–780.
Rights and permissions
About this article
Cite this article
Magedov, I.V., Shapakin, S.Y., Drozd, V.N. et al. 2,2,3,3-Tetracyano-7,8-dithiabicyclo[3.2.1]octanes: Structural studies. Chem Heterocycl Compd 30, 674–682 (1994). https://doi.org/10.1007/BF01166308
Issue Date:
DOI: https://doi.org/10.1007/BF01166308