Chemistry of Heterocyclic Compounds

, Volume 30, Issue 6, pp 674–682 | Cite as

2,2,3,3-Tetracyano-7,8-dithiabicyclo[3.2.1]octanes: Structural studies

  • I. V. Magedov
  • S. Yu. Shapakin
  • V. N. Drozd
  • A. S. Batsanov
  • D. S. Yufit
  • Yu. T. Struchkov


2,2,3,3-Tetracyano-7,8-dithiabicyclo[3.2.1]octanes were formed in the reaction of dithiocarboxyclic acid allyl and cinnamyl esters with tetracyanoethylene, and their structure was determined by a number of physico-chemical methods, including x-ray structural study.


Ester Organic Chemistry Octane Allyl Structural Study 
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  1. 1.
    I. V. Magedov, V. N. Drozd, S. Yu. Shapakin, D. S. Yufit, and Yu. T. Struchkov, Sulfur Lett., 17 (1994).Google Scholar
  2. 2.
    F. H. Allen, O. Kennard, D. G. Watson, L Brummer, A. G. Orpen and R. Taylor, J. Chem. Soc. Perkin II. No. 1, 1(1987).Google Scholar
  3. 3.
    H. Gotthardt, O. M. Huss, and S. Schog-Tribbensee, Chem. Ber.,114, 285 (1981).Google Scholar
  4. 4.
    B. Kojic-Prodic, Z. Ruzic-Toros, and J. J. Herak, Acta Crystallogr.,B37, 214 (1981).Google Scholar
  5. 5.
    I. R. Fjeldskaar, D. Grace, C. Romming, and L. Scattebol, Acta Chem. Scand.,B42, 280 (1988).Google Scholar
  6. 6.
    C. A. G. Haasnoot, F. A. A. M. de Leeuw, and C. Altona, Tetrahedron,36, 2783 (1900).Google Scholar
  7. 7.
    N. L. Allinger and J. T. Sprague, J. Am. Chem. Soc.,95, 3893 (1973).Google Scholar
  8. 8.
    J. Kao and N. L. Allinger, J. Am. Chem. Soc.,99, 975 (1977).Google Scholar
  9. 9.
    H. Günther, Introduction m NMR Spectroscopy [Russian translation], Mir, Moscow (1984), pp. 132, 404.Google Scholar
  10. 10.
    G. M. Sheldrick, SHELXTL PLUS. PC Version, Siemens Analytical X-ray Instruments, Inc., Madison, Wisconsin (1989).Google Scholar

Copyright information

© Plenum Publishing Corporation 1995

Authors and Affiliations

  • I. V. Magedov
  • S. Yu. Shapakin
  • V. N. Drozd
  • A. S. Batsanov
  • D. S. Yufit
  • Yu. T. Struchkov

There are no affiliations available

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