Chemistry of Heterocyclic Compounds

, Volume 32, Issue 9, pp 1066–1074 | Cite as

Synthesis and properties of N-methylmorpholinium 4aryl-6-methyl-5-phenylcarbamoyl-3cyano-1,4dihydropyridine-2-thiolates. Molecular and crystalline structure of 2allylthio-6-methyl-5-phenylcarbamoyl-4-(2chlorophenyl)-3-cyano-1,4-dihydropyridine

  • V. D. Dyachenko
  • S. G. Krivokolysko
  • V. N. Nesterov
  • V. P. Litvinov


By the condensation of an aromatic aldehyde, the anilide of acetoacetic acid, cyanothioacetamide, and Nmethylmorpholine, substituted N-methylmorpholinium 1,4-dihydropyridine-2-thiolates have been synthesized and subsequently used in the synthesis of the corresponding thiones, 2-alkylthiopyridines, thieno[2, 3b]pyridines, and disulfides. X-ray diffraction has been used to establish the structure of 2-allylthio-6-methyl-5phenylcarbamoyl-4-(2-chlorophenyl)-3-cyano-1, 4-dihydropyridine.


Organic Chemistry Aldehyde Pyridine Disulfide Crystalline Structure 
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Copyright information

© Plenum Publishing Corporation 1997

Authors and Affiliations

  • V. D. Dyachenko
  • S. G. Krivokolysko
  • V. N. Nesterov
  • V. P. Litvinov

There are no affiliations available

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