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Synthesis and study of the pmr spectra of 1,10,11,20-tetrahydrodipyrazolo [3,4-f:3′,4′-m]dipyrido[2,3-c:2′,3′-j][1,2,5,8,9,12]-hexaazacyclotetradecene derivatives

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Chemistry of Heterocyclic Compounds Aims and scope

Abstract

1,10,11,20-Tetrahydropyrazolo[3,4-f:3′,4′-m]dipyrido[2,3-c:2′,3′-j][1,2,5,8,9,-12] hexaazacyclotetradecene derivatives were obtained by the reaction of nickel nitrate, palladium chloride, potassium tetrachloroplatinate, or copper sulfate with 5-amino-3-methyl-4-(2-chloro-3-pyridylazo)-1-R-pyrazoles in dimethylformamide in the presence of potassium carbonate and were characterized by the results of elementary analysis and data from the IR, UV, PMR, and mass spectra.

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Translated from Khimiya Geterotsiklicheskikh Soedinenii, No. 5, pp. 701–706, May, 1979.

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Dziomko, V.M., Berestevich, B.K., Kessenikh, A.V. et al. Synthesis and study of the pmr spectra of 1,10,11,20-tetrahydrodipyrazolo [3,4-f:3′,4′-m]dipyrido[2,3-c:2′,3′-j][1,2,5,8,9,12]-hexaazacyclotetradecene derivatives. Chem Heterocycl Compd 15, 572–577 (1979). https://doi.org/10.1007/BF00773230

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  • DOI: https://doi.org/10.1007/BF00773230

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