Skip to main content
SpringerLink
Log in

Synthesis of 2,5′-substituted 2′,5-bipyrimidines

  • Published:
Chemistry of Heterocyclic Compounds Aims and scope

Abstract

Reaction of 5-substituted-2-methylpyrimidines with the Vilsmeyer complex followed by condensation of the resulting immonium salts and acroleins with aromatic amidines has given liquid crystalline 2′,5-bipyrimidines.

This is a preview of subscription content, log in via an institution to check access.

Access this article

Log in via an institution

Price excludes VAT (USA)
Tax calculation will be finalised during checkout.

Instant access to the full article PDF.

Institutional subscriptions

Similar content being viewed by others

Literature Cited

  1. T. Kobayashi, J. Kawashima, T. Tabohashi, T. Sakurai, R. Higuchi, E. Komatsu, and K. Takeuchi, Eur. Pat. Appl. 225,195;Chem. Abstr. 107, 124,754 (1987).

    Google Scholar 

  2. M. Schadt, R. Buchecker, F. Leenhout, A. Boller, A. Villiger, and M. Petrzilka,Mol. Cryst. Liq. Cryst. 139, 1 (1986).

    Google Scholar 

  3. H. Suenaga, M. Taguchi, and T. Harada, Kokai Tokkyo Koho 61-215,373 (Jpn.),Chem. Abstr. 106, 205,380 (1987).

    Google Scholar 

  4. K. Bofinger, R. Eidenschink, R. Hittich, R. Hopf, J. Dr. Krause, A. Pausch, V. Reiffenrath, B. S. Scheuble, and A. Waechtler, Ger. Offen. 3,518,734 DE;Chem. Abstr. 106, 93,679c (1987).

    Google Scholar 

  5. Japanese Patent No. 60-25,973;Ref. Zh. Khim., 24N241P (1985).

  6. N. Yoshida, K. Kitano, Y. Furukawa, T. Ogawa, S. Sugimori, Y. Goto, T. Isoyama, and K. Nigorikawa, Eur. Pat. Appl. No. 186,045 EP;Chem. Abstr. 105, 181–666 (1986).

    Google Scholar 

  7. N. Kitano, T. Ogawa, Y. Furukawa, and N. Yoshida, Kokai Tokkyo Koho 61-33,177;Chem. Abstr. 105, 105,921 (1986).

    Google Scholar 

  8. Y. Kitano, T. Ogawa, Y. Goto, and N. Yoshida, Kokai Tokkyo Koho 60-172,971;Chem. Abstr. 104, 88,588 (1986).

    Google Scholar 

  9. Y. Kitano, T. Ogawa, Y. Goto, and N. Yoshida, Kokai Tokkyo Koho 60-190,766;Chem. Abstr. 104, 148,898 (1986).

    Google Scholar 

  10. V. P. Mamaev, M. A. Mikhaleva, and A. I. Shadrina,Khim. Geterotsikl. Soedin., No. 3, 371 (1988).

    Google Scholar 

  11. V. P. Mamaev and O. A. Zagulyaeva,Khim. Geterotsikl. Soedin., Coll. 1, 354 (1967).

    Google Scholar 

  12. H. Zaschke, S. Arndt, V. Wagner, and H. Schubert,Z. Chem. 17, 293 (1977).

    Google Scholar 

  13. H. Yamanaka and T. Sakamoto,J. Synth. Org. Chem. 43, 951 (1985).

    Google Scholar 

  14. T. Koyama, T. Hirota, C. Basho, Y. Watanabe, Y. Kitauchi, Y. Satoh, S. Ohmori, and M. Yamato,Chem. Pharm. Bull. 24, 1459 (1976).

    Google Scholar 

  15. T. Hirota, T. Koyama, C. Basho, T. Nanba, K. Sasaki, and M. Yamato,Chem. Pharm. Bull. 25, 3056 (1977).

    Google Scholar 

  16. Z. Arnold and F. Sorm,Coll. Czech. Chem. Commun. 23, 452 (1958).

    Google Scholar 

  17. D. Demus and H. Zaschke,Flüssige Kristalle in Tabellen, Deutscher Verlag für Grundstofindustrie (1974), p. 230.

  18. H. Schubert, H.-J. Lorenz, R. Hoffmann, and F. Franke,Z. Chem. 6, 337 (1966).

    Google Scholar 

  19. C. Jutz, R. Kirchlechner, and H.-J. Seidel,Chem. Ber. 102, 2301 (1969).

    Google Scholar 

  20. M. A. Mikhaleva, V. A. Savel'ev, A. I. Pavlyuchenko, M. F. Grebenkin, and V. P. Mamaev,Khim. Geterotsikl. Soedin., No. 9, 1228 (1986).

    Google Scholar 

  21. R. Dabrowski, J. Dziaduszek, T. Szczucinski, W. Drzewinski, Z. Stolarz, J. Zmija, J. Parka, and B. Sosnowska, Eur. Pat. Appl. 227,004;Chem. Abstr. 107, 187,658p (1987).

    Google Scholar 

  22. M. A. Mikhaleva, G. A. Kolesnichenko, K. I. Rubina, Yu. Sh. Gol'dberg, V. A. Savel'ev, L. Ya. Leitis, M. V. Shimanskaya, and V. P. Mamaev,Khim. Geterotsikl. Soedin., No. 3, 380 (1986).

    Google Scholar 

Download references

Author information

Authors and Affiliations

  1. Novosibirsk Institute of Organic Chemistry, Siberian Branch, Academy of Sciences of the USSR, 630090, Novosibirsk

    M. A. Mikhaleva, T. A. Kizner & V. P. Mamaev

Authors
  1. M. A. Mikhaleva
    View author publications

    You can also search for this author in PubMed Google Scholar

  2. T. A. Kizner
    View author publications

    You can also search for this author in PubMed Google Scholar

  3. V. P. Mamaev
    View author publications

    You can also search for this author in PubMed Google Scholar

Additional information

Deceased.

Translated from Khimiya Geterotsiklicheskikh Soedinenii, No. 6, pp. 804–807, June, 1990.

Rights and permissions

Reprints and permissions

About this article

Cite this article

Mikhaleva, M.A., Kizner, T.A. & Mamaev, V.P. Synthesis of 2,5′-substituted 2′,5-bipyrimidines. Chem Heterocycl Compd 26, 671–674 (1990). https://doi.org/10.1007/BF00756421

Download citation

  • Received:

  • Issue Date:

  • DOI: https://doi.org/10.1007/BF00756421

Keywords

Search

Navigation