Skip to main content
SpringerLink
Log in

Two-dimensional NMR spectra of 17α-(1-aziridinylmethyl)-5α-androstan-17β-ol

  • Published:
Chemistry of Heterocyclic Compounds Aims and scope

Abstract

The complex1H and13C NMR spectra of 17α-(1-aziridinylmethyl)-5α-androstan-17β-ol were analyzed using two-dimensional (2M) spectroscopy. The configuration of the substituents at the 17 position was determined using the 2M-spectroscopy of the nuclear Overhauser effect. The direct13C-13C SSCCs were determined.

This is a preview of subscription content, log in via an institution to check access.

Access this article

Log in via an institution

Price excludes VAT (USA)
Tax calculation will be finalised during checkout.

Instant access to the full article PDF.

Institutional subscriptions

Similar content being viewed by others

Literature Cited

  1. J. B. Jones and J. D. Leman, Can. J. Chem.,49, 2420 (1971).

    Google Scholar 

  2. J. W. Blunt and J. B. Stothers, Org. Magn. Reson.,9, 439 (1977).

    Google Scholar 

  3. E. L. Eliel and K. M. Pietrusiewicz, Topics in13C NMR Spectroscopy, Vol. 3 (1979), p. 371.

    Google Scholar 

  4. G. A. Morris, Magn. Reson. Chem.,24, 371 (1986).

    Google Scholar 

  5. H.-J. Schneider, U. Bucheit, N. Becker, G. Schmidt, and U. Siehl, J. Am. Chem. Soc.,107, 7027 (1985).

    Google Scholar 

  6. A. Bax and R. Freeman, J. Magn. Reson.,44, 542 (1981).

    Google Scholar 

  7. A. Bax, R. Freeman, and T. A. Frenkiel, J. Am. Chem. Soc.,103, 2102 (1981).

    Google Scholar 

  8. D. L. Turner, J. Magn. Reson.,49, 175 (1982).

    Google Scholar 

  9. A. Bax, R. Freeman, and S. P. Kempsell, J. Magn. Reson.,41, 3449 (1980).

    Google Scholar 

  10. S. Macura, K. Wüthrich, and R. R. Ernst, J. Magn. Reson.,46, 269 (1982).

    Google Scholar 

Download references

Author information

Authors and Affiliations

  1. P. Lumumba Peoples' Friendship University, 117923, Moscow

    A. é. Aliev, A. A. Fomichev, A. N. Sova, I. M. Gella & R. G. Kostyanovskii

  2. Khar'kov Scientific Research Institute of the Endocrinology and Chemistry of Hormones, 310002, Khar'kov

    A. é. Aliev, A. A. Fomichev, A. N. Sova, I. M. Gella & R. G. Kostyanovskii

  3. Institute of Chemical Physics, Academy of Sciencies of the USSR, 117977, Moscow

    A. é. Aliev, A. A. Fomichev, A. N. Sova, I. M. Gella & R. G. Kostyanovskii

Authors
  1. A. é. Aliev
    View author publications

    You can also search for this author in PubMed Google Scholar

  2. A. A. Fomichev
    View author publications

    You can also search for this author in PubMed Google Scholar

  3. A. N. Sova
    View author publications

    You can also search for this author in PubMed Google Scholar

  4. I. M. Gella
    View author publications

    You can also search for this author in PubMed Google Scholar

  5. R. G. Kostyanovskii
    View author publications

    You can also search for this author in PubMed Google Scholar

Additional information

Translated from Khimiya Geterotsiklicheskikh Soedinenii, No. 11, pp. 1466–1471, November, 1988.

Rights and permissions

Reprints and permissions

About this article

Cite this article

Aliev, A.é., Fomichev, A.A., Sova, A.N. et al. Two-dimensional NMR spectra of 17α-(1-aziridinylmethyl)-5α-androstan-17β-ol. Chem Heterocycl Compd 24, 1212–1216 (1988). https://doi.org/10.1007/BF00633497

Download citation

  • Received:

  • Issue Date:

  • DOI: https://doi.org/10.1007/BF00633497

Keywords

Search

Navigation