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Identification of aliphatic 2- and 3-hydroxy acids in the form of cyclic phenylboronates by GLC-mass spectrometry

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Abstract

A method is prepared for identifying aliphatic 2- and 3-hydroxy acids which is based on the GLC-mass spectrometry of the corresponding phenylboronates. The phenyl-boronates are sufficiently volatile for analysis with the aid of GLC and give simple and informative mass spectra.

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Literature cited

  1. Bacterial Lipopolysaccharides, E. H. Kass and S. M. Wolff, eds., University Press, Chicago (1973).

    Google Scholar 

  2. C. Hitchcock, Biochem. J.,103, 8P (1967).

  3. A. Ya. Veinberg, L. A. Vakulova, and G. I. Samokhvalov, Usp. Khim.,35, 2072 (1966).

    Article  CAS  Google Scholar 

  4. S. G. Batrakov and L. D. Bergelson, Chem. Phys. Lipids,21, 1 (1978).

    Article  CAS  PubMed  Google Scholar 

  5. I. Yano, Y. Furukawa, and M. Kusunose, FEBS Lett.,4, 96 (1969).

    Article  CAS  PubMed  Google Scholar 

  6. C. W. Moss and S. B. Dees, J. Chromatogr.,112, 595 (1975).

    Article  CAS  Google Scholar 

  7. J. S. O'Brien and G. Rouser, Anal. Biochem.,7, 288 (1964).

    Article  CAS  PubMed  Google Scholar 

  8. R. D. Wood, P. K. Raju, and R. Reiser, J. Am. Oil. Chem. Soc.,42, 81 (1965).

    Article  CAS  Google Scholar 

  9. R. A. Laine, N. D. Young, J. N. Gelber, and C. C. Sweeley, Biomed. Mass Spectrom.,1, 10 (1974).

    Article  CAS  PubMed  Google Scholar 

  10. R. Ryhage and E. Stenhagen, Ark. Kem.,15, 545 (1960).

    CAS  Google Scholar 

  11. C. F. Poole and A. Zlatkis, J. Chromatogr.,184, 99 (1980).

    Article  CAS  Google Scholar 

  12. S. G. Batrakov, A. N. Ushakov, and V. L. Sadovskaya, Bioorg. Khim.,2, 1095 (1976).

    CAS  Google Scholar 

  13. C. J. W. Brooks and J. Maclean, J. Chromatogr. Sci.,9, 19 (1971).

    Article  Google Scholar 

  14. I. R. McKinley and H. Weigel, Chem. Commun., 1022 (1970).

  15. I. R. McKinley and H. Weigel, Chem. Commun., 1051 (1972).

  16. S. G. Batrakov, E. F. Il'ina, B. V. Rozynov, V. L. Sadovskaya, and L. D. Bergel'son, Izv. Akad. Nauk SSSR, Ser. Khim., 821 (1975).

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M. M. Shemyakin Institute of Bioorganic Chemistry, Moscow. Translated from Khimiya Prirodnykh Soedinenii, No. 3, pp. 283–288, May–June, 1981.

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Batrakov, S.G., Rozynov, B.V. & Ushakov, A.N. Identification of aliphatic 2- and 3-hydroxy acids in the form of cyclic phenylboronates by GLC-mass spectrometry. Chem Nat Compd 17, 213–217 (1981). https://doi.org/10.1007/BF00568504

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  • DOI: https://doi.org/10.1007/BF00568504

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