Abstract
The reaction of 3-methyl-3-buten-1-ol with acetophenone and benzalacetone affords a mixture of isomeric 2-methyl-2-aryldi- and tetrahydropyrans, the composition of which was ascertatined by chromatography-mass spectromety.
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Literature Cited
E. Hanshke, Chem. Ber., 88, 1053 (1955).
R, Helin, R. Henry, and S. Gelin, C. R. Acad. Sci., 273, 254 (1971).
A. A. Gevorkyan, A. S. Arakelyan, and P. I. Kazaryan, Khim. Geterotsikl. Soedin., No. 12, 1611 (1982).
A. A. Gevorkyan, A. S. Arakelyan, and N. M. Khizyantsyan, Arm. Khim. Zh., No. 9, 743 (1977).
P. H. Williams, G. G. Ecke, and S. A. Ballard, J. Am. Chem. Soc., 72, 5738 (1950).
U. G. Ibatullin, Yu. N. Popov, I. R. Kleinos, and M. G. Safarov, Manuscript Deposited at the Branch of the Scientific-Research Institute of Technicoeconomic Research of the Ministry of the Chemical Industry of the USSR, July 24, 1984 [in Russian], No. 701 khp-D 84.
Weygand-Hilgetag, Experimental Methods in Organic Chemistry [Russian translation], Khimiya, Moscow (1969), p. 183.
N. A. Akmanova, R. F. Sagitdinova, R. F. Taipov, and V. P. Yur'ev, Zh. Org. Khim., 16, 2309 (1980).
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Translated from Khimiya Geterotsiklicheskikh Soedinenii, No. 7, pp. 883–885, July, 1986.
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Ibatullin, U.G., Petrushina, T.F., Nurtdinova, Z.M. et al. Condensation of 3-methyl-3-buten-1-ol with some ketones. Chem Heterocycl Compd 22, 700–702 (1986). https://doi.org/10.1007/BF00522725
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DOI: https://doi.org/10.1007/BF00522725