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Mass-spectrometric behavior and PMR spectra of 9-(2-R-1,3-dioxan-5-yl)purines

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Chemistry of Heterocyclic Compounds Aims and scope

Abstract

A trans configuration with an axial orientation of both the purine ring and the furyl ring or the ethoxy group in the 2 position of the dioxane residue was established by PMR spectroscopy for 9-(2-furyl-1,3-dioxan-5-yl)- and 9-(2-ethoxy-2-methyl-1,3-dioxan-5-yl)purine. A comparative analysis of the mass spectra of these compounds makes it possible to confirm conclusions regarding their stereochemistry drawn on the basis of the PMR spectra.

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Literature cited

  1. A. F. Mishnev, Ya. Ya. Bleidelis, É. É. Liepin'sh, N. P. Ramzaeva, and I. N. Goncharova, Khim. Geterotsikl. Soedin., No. 7, 976 (1979).

    Google Scholar 

  2. Yu. Yu. Samitov, I. N. Goncharova, N. P. Ramzaeva, A. F. Mishnev, and Ya. Ya. Bleidelis, Khim. Geterotsikl. Soedin., No. 11, 1523 (1981).

    Google Scholar 

  3. V. G. Zaikin and N. S. Vul'fson, Khim. Geterotsikl. Soedin., No. 11, 1443 (1978).

    Google Scholar 

  4. A. Mandelbaum, Mass Spectrometry Rev., 2, 223 (1983).

    Google Scholar 

  5. J. Reuben, Prog. NMR Spectrosc., 9, 7 (1973).

    Google Scholar 

  6. Yu. Yu. Samitov, Atlas of the NMR Spectra of Spatial Isomers [in Russian], Vol. 1, Izd. Kazansk. Univ. (1978), p. 100.

    Google Scholar 

  7. N. A. Klyuev, I. S. Shpileva, L. I. Medvedeva, G. N. Lyapunova, and N. P. Bednyagina, Khim. Geterotsikl. Soedin., No. 11, 1506 (1981).

    Google Scholar 

  8. I. L. Holmes and F. P. Lossing, Org. Mass Spectrom., 14, 512 (1979).

    Google Scholar 

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Authors and Affiliations

  1. Institute of Organic Synthesis, Academy of Sciences of the Latvian SSR, 226006, Riga

    Yu. Yu. Samitov, I. N. Goncharova, N. P. Ramzaeva & P. B. Terent'ev

Authors
  1. Yu. Yu. Samitov
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  2. I. N. Goncharova
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  3. N. P. Ramzaeva
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  4. P. B. Terent'ev
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Additional information

Translated from Khimiya Geterotsiklicheskikh Soedinenii, No. 5, pp. 691–696, May, 1984.

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Samitov, Y.Y., Goncharova, I.N., Ramzaeva, N.P. et al. Mass-spectrometric behavior and PMR spectra of 9-(2-R-1,3-dioxan-5-yl)purines. Chem Heterocycl Compd 20, 558–564 (1984). https://doi.org/10.1007/BF00514312

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  • DOI: https://doi.org/10.1007/BF00514312

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