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N-Glycosides. 4. Synthesis of 3-glycosyl-4-hydroxyhexahydropyrimidine-2-thiones on the basis of glycosyl isothiocyanates

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Chemistry of Heterocyclic Compounds Aims and scope

Abstract

The reaction of peracetylgluco(galacto)pyranosyl isothiocyanates with β-aminopropionaldehyde diethylacetal gave the corresponding glycosylthioureas, which, after removal of the protective groups, are converted spontaneously to 3-gluco(galacto)pyranosyl-4-hydroxyhexahydropyrimidine-2-thiones.

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Authors and Affiliations

  1. M. V. Lomonosov Moscow Institute of Fine Chemical Technology, 119831, Moscow

    A. D. Shutalev, L. A. Ignatova & B. V. Unkovskii

Authors
  1. A. D. Shutalev
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  2. L. A. Ignatova
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  3. B. V. Unkovskii
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Additional information

See [1] for communication 3.

Translated from Khimiya Geterotsiklicheskikh Soedinenii, No. 4, pp. 548–551, April, 1984.

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Shutalev, A.D., Ignatova, L.A. & Unkovskii, B.V. N-Glycosides. 4. Synthesis of 3-glycosyl-4-hydroxyhexahydropyrimidine-2-thiones on the basis of glycosyl isothiocyanates. Chem Heterocycl Compd 20, 447–450 (1984). https://doi.org/10.1007/BF00513866

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  • DOI: https://doi.org/10.1007/BF00513866

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