Abstract
2-Alkoxycarbonylmethyl-1,3-oxathiolane and -dithiolane, 3-methyloxycarbonylmethyl-7,8-dimethyl-1,5-dihydrobenzo[e]-1,3-dithiepine, and 2-methoxycarbonylmethyl-1,3-dithiolo[4,5-b]quinoxaline were synthesized on the basis of the reaction of esters of propiolic acid with β-mercaptoethanol, 1,2-dimercaptoethanol, 1,2-dimethyl-4,5-di(mercaptomethyl)benzene, and 2,3-dimercaptoquinoxaline in chloroform medium in the presence of K2CO3 or in DMSO medium.
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Translated from Khimiya Geterotsilicheskikh Soedinenii, No. 8, pp. 1062–1065, August, 1984.
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Elokhina, V.N., Nakhmanovich, A.S., Karnaukhova, R.V. et al. Reaction of propiolic acid esters with dithiols and β-mercaptoethanol. Chem Heterocycl Compd 20, 862–865 (1984). https://doi.org/10.1007/BF00513570
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DOI: https://doi.org/10.1007/BF00513570