Abstract
The condensation of 2,3-0-isopropylideneribofuranosylamine tosylate with 4-methyl-4-isothiocyanato-2-pentanone in the presence of bases was studied. In pyridine the reaction gives a mixture of 3-(2′,3′-0-ispropylidene-β-D-ribofuranosyl)-4,6,6-trimethyl-1,2,3,6-tetrahydropyrimidine-2-thione and 3-(2′,3′-0-isopropylidene-β-D-ribofuranosyl)-4-methylene-6,6-dimethylhexahydropyrimidine-2-thione.
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A. D. Shutalev, L. A. Ignatova, and B. V. Unkovskii, Khim. Geterotsikl. Soedin., No. 6, 825 (1982).
N. J. Cusack, B. J. Hildich, D. H. Robinson, P. W. Rugg, and G. A. Shaw, J. Chem. Soc., Perkin Trans. I, No. 16, 1720 (1973).
O. S. Bhanot, N. K. Ralhan, and K. S. Narang, Indian J. Chem., 2, 238 (1964).
G. Zigeuner, W.-B. Lintschinger, A. Fuchsgruber, and K. Kollmann, Monatsh. Chem., 107, 155 (1976).
M. J. Janssen, Rec. Trav. Chim., 79, 1066 (1960).
R. K. Ritchie and H. Spedding, Spectrochim. Acta, 26A, 9 (1970).
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See [1] for communication 2.
Translated from Khimiya Geterotsiklicheskikh Soedinenii, No. 2, pp. 244–246, February, 1984.
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Shutalev, A.D., Ignatova, L.A. & Unkovskii, B.V. N-glycosides. 3. Reaction of 2,3-0-isopropylideneribofuranosylamine tosylate with 4-methyl-4-isothiocyanato-2-pentanone. Chem Heterocycl Compd 20, 201–203 (1984). https://doi.org/10.1007/BF00506293
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DOI: https://doi.org/10.1007/BF00506293