Abstract
The corresponding five benzothiolactams were obtained by cyclization of racemic arylalkyl isothiocyanates in polyphosphoric acid. The fragmentation of all five pairs of isomeric compounds under the influence of electron impact was investigated thoroughly.
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V. M. Potapov, V. M. Dem'yanovich, L. D. Solov'eva, and O. E. Vendrova, Khim. Geterotsikl. Soedin., No. 1, 94 (1976).
V. M. Potapov, V. M. Dem'yanovich, L. D. Solov'eva, and O. E. Vendrova, Dokl. Akad. Nauk SSSR, 241, 592 (1978).
A. Kjaer, M. Ohashi, J. Wilson, and C. Djerassi, Acta Chem. Scand., 17, 2143 (1963).
A. Kjaer and W. Wagmeres, Acta Chem. Scand., 19, 1985 (1965).
E. Bach, A. Kjaer, R. Shapiro, and C. Djerassi, Acta Chem. Scand., 19, 2438 (1965).
F. Larsson, S. Lawesson, I. Moller, and G. Schroll, Acta Chem. Scand., 27, 747 (1973).
P. B. Terent'ev, L. D. Solov'eva, V. M. Dem'yanovich, O. A. Popova, and V. M. Potapov, Khim. Geterotsikl. Soedin., No. 2, 246 (1979).
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Translated from Khimiya Geterotsiklicheskikh Soedinenii, No. 11, pp, 1520–1523, November, 1980.
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Terent'ev, P.B., Vendrova, O.E., Solov'eva, L.D. et al. Mass-spectral behavior of benzothiolactams and isomeric ω-arylalkyl isothiocyanates. Chem Heterocycl Compd 16, 1157–1160 (1980). https://doi.org/10.1007/BF00504114
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DOI: https://doi.org/10.1007/BF00504114