Skip to main content
SpringerLink
Log in

Synthesis and study of heteroaromatic ligands containing a pyrimidine ring

  • Published:
Chemistry of Heterocyclic Compounds Aims and scope

Abstract

5-Hexyl-3-[2-(1H-pyrazol-1-yl)pyrimidin-4-yl]amino-1(2)H-1,2,4-triazoles and 2-(3,5-dipropyl-4-ethyl-1H-pyrazol-1-yl)-6-methyl-4-(5-methyl-1H-pyrazol-1-yl)-aminopyrimidine were synthesized by the reaction of 4-chloropyrimidines with 3-araino-5-hexyl-1H-1,2,4-triazole and 3-amino-5-methyl-1H-pyrazole. Their IR, UV, and PMR spectra were investigated. New methods for the preparation of the intermediates, viz., 2-hydrazino-4(3H)-pyrimidinones and 2-(1H-pyrazol-1-yl)-4(3H)-pyrimidinones, that make it possible to obtain these compounds in higher yields are described.

This is a preview of subscription content, log in via an institution to check access.

Access this article

Log in via an institution

Price excludes VAT (USA)
Tax calculation will be finalised during checkout.

Instant access to the full article PDF.

Institutional subscriptions

Similar content being viewed by others

Literature cited

  1. A. V. Ivashchenko, O. N. Garicheva, L. V. Shmelev, and Yu. S. Ryabokobylko, Khim. Geterotsikl. Soedin., No. 8, 1114 (1980).

    Google Scholar 

  2. A. V. Ivashchenko, O. N. Garicheva, A. P. Bogdanov, and V. M. Dziomko, Summaries of Papers Presented at the 13th All-Union Chugaev Conference on the Chemistry of Complexes [in Russian], Nauka (1978), p. 160.

  3. K. Shirakawa, J. Pharm. Soc. Jpm., 73, 635 (1953); No. 24, 78184 (1956).

    Google Scholar 

  4. K. Shirakawa and T. Tsujikawa, Takeda Kenkyusho Mempo, l22, 19 (1963); Chem. Abstr., 60, 12009b (1964).

    Google Scholar 

  5. A. V. Ivashchenko and V. M. Dziomko, Khim. Geterotsikl. Soedin., No. 9, 1255 (1977).

    Google Scholar 

  6. F. Baumhoch, H. G. Henning, and G. Hilgetag, Z. Chem., 4, 67 (1964).

    Google Scholar 

  7. A. V. Spasov and Z. D. Raikov, Z. Chem., 17, 260 (1971).

    Google Scholar 

  8. E. Alcade, J. De Mendaza, and J. Almera, J. Heterocycl. Chem., 11, 423 (1974).

    Google Scholar 

  9. M. Atkinson, A. A. Komzak, E. A. Parkes, and J. B. Polya, J. Chem. Soc., No. 12, 4508 (1954).

    Google Scholar 

Download references

Author information

Authors and Affiliations

  1. Scientific-Research Institute of Organic Intermediates and Dyes, 103787, Moscow

    A. V. Ivashchenko, O. N. Garicheva, L. V. Shmelev, Yu. S. Ryabokobylko & G. M. Adamova

  2. All-Union Scientific-Research Institute of Chemical Reagents and Ultrapure Chemical Substances, 107258, Moscow

    A. V. Ivashchenko, O. N. Garicheva, L. V. Shmelev, Yu. S. Ryabokobylko & G. M. Adamova

Authors
  1. A. V. Ivashchenko
    View author publications

    You can also search for this author in PubMed Google Scholar

  2. O. N. Garicheva
    View author publications

    You can also search for this author in PubMed Google Scholar

  3. L. V. Shmelev
    View author publications

    You can also search for this author in PubMed Google Scholar

  4. Yu. S. Ryabokobylko
    View author publications

    You can also search for this author in PubMed Google Scholar

  5. G. M. Adamova
    View author publications

    You can also search for this author in PubMed Google Scholar

Additional information

Translated from Khimiya Geterotsiklicheskikh Soedinenii, No. 12, pp. 1673–1677, December, 1980.

Rights and permissions

Reprints and permissions

About this article

Cite this article

Ivashchenko, A.V., Garicheva, O.N., Shmelev, L.V. et al. Synthesis and study of heteroaromatic ligands containing a pyrimidine ring. Chem Heterocycl Compd 16, 1271–1275 (1980). https://doi.org/10.1007/BF00501833

Download citation

  • Received:

  • Issue Date:

  • DOI: https://doi.org/10.1007/BF00501833

Keywords

Search

Navigation