Synthesis and alkylation of 9-ethoxy-1H-pyrrolo[3,2-b]quinoline
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9-Ethoxy-1H-pyrrolo[3,2-b]quinoline has been synthesized by the hydrogenation of 2-[2-(N,N-dimethylamino)vinyl]-3-nitro-4-ethoxyquinoline using Raney nickel. Alkylation using N,N-dimethylchloroethylamine and hydrolysis with HBr gave two isomers whose structures were established using PMR and mass spectrometry.
KeywordsHydrogenation Nickel Hydrolysis Mass Spectrometry Organic Chemistry
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