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Formation of thienothiophenes in the high temperature reaction of 2-chlorothiophene with compounds containing the c2h5s group

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Chemistry of Heterocyclic Compounds Aims and scope

Abstract

The high temperature gas-phase reaction of 2-chlorothiophene with a mixture of diethyl disulfide and diethyl trisulfide constitutes a simple one-step synthesis of a 4∶1 mixture of thieno[2,3-b]- and thieno[3,2-b]-thiophenes. Their total yield depends on the nature of the donor of the ethylthio group.

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Authors and Affiliations

  1. Irkutsk Institute of Organic Chemistry, Siberian Branch, Academy of Sciences of the USSR, 664033, Irkutsk

    N. A. Korchevin, é. N. Sukhomoazova, L. P. Turchaninova, G. G. Efremova, N. A. Kalinina, é. N. Deryagina & M. G. Voronkov

Authors
  1. N. A. Korchevin
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  2. é. N. Sukhomoazova
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  3. L. P. Turchaninova
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  4. G. G. Efremova
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  5. N. A. Kalinina
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  6. é. N. Deryagina
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  7. M. G. Voronkov
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Additional information

Communication 30 of the series “High temperature organic synthesis”. For Communication 29, see [1].

Translated from Khimiya Geterotsiklicheskikh Soedinenii, No. 8, pp. 1041–1044, August, 1988.

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Korchevin, N.A., Sukhomoazova, é.N., Turchaninova, L.P. et al. Formation of thienothiophenes in the high temperature reaction of 2-chlorothiophene with compounds containing the c2h5s group. Chem Heterocycl Compd 24, 857–860 (1988). https://doi.org/10.1007/BF00479335

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  • DOI: https://doi.org/10.1007/BF00479335

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