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Synthesis of some O,O-diethyl S-(β-acylaminoethyl) dithiophosphates

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Chemistry of Heterocyclic Compounds Aims and scope

Abstract

The ethyleneimides of N-phthalyl-D,L-valine, N-phthalyl-D,L-glycine, N-phthalyl-D,L-alanine, N-carbobenzoxy-D,L-valine, N-benzoyl-D,L-leucine, and of the γ-methyl ester of N-carbobenzoxy-L-glutamic acid and monomethyl succinate were synthesized. A number of O,O-diethyl S-(β-acrylaminoethyl) dithiophosphates were obtained by opening the ethyleneimine ring in the ethyleneimides of N-acylated amino acids with diethyl dithiophosphoric acid. The β-chloroethylamides of phthalyl-D,L-valine, N-acetyl-D,L-valine, and monomethyl succinate were obtained.

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Translated from Khimiya Geterotsiklicheskikh Soedinenii, No. 4, pp. 479–482, April, 1972.

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Yamontaite, A.A., Krasil'nikova, G.K., Kil'disheva, O.V. et al. Synthesis of some O,O-diethyl S-(β-acylaminoethyl) dithiophosphates. Chem Heterocycl Compd 8, 436–439 (1972). https://doi.org/10.1007/BF00477417

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  • DOI: https://doi.org/10.1007/BF00477417

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