Abstract
Procedures have been developed for the synthesis of 1,4-dihydropyridine-3,5-dicarbothionic acid S-esters via the direct thiolysis of 1,4-dihydropyridine-3,5-dicarboxylic acids and their ester derivatives. The use of different acid activating agents and thiolysis agents is discussed.
Similar content being viewed by others
Literature Cited
B. A. Vigante, Ya. Ya. Ozols, G. Ya. Dubur, Yu. I. Beilis, E. M. Belash, and V. V. Prezhdo, Khim. Geterotsikl. Soedin., No. 2, 219 (1982).
B. A. Vigante, Ya. Ya. Ozols, R. O. Vitolinya, A. A. Kimenis, and G. Ya. Dubur, USSR Inventor's Certificate No. 798,100; Byull. Izobret., No. 3, 81 (1981).
V. A. Vigante, Ya. Ya. Ozols, G. O. Silenietse, and A. A. Kimenis, USSR Inventor's Certificate No. 794,006; Byull. Izobret., No. 1, 94 (1981).
H.-J. Liu and S. J. Sabesan, Can. J. Chem., 58, 2645 (1980).
B. Neises and W. Steglich, Angew. Chem., Int. Ed., No. 7, 522 (1978).
T. Mukaiyama, T. Takeda, and K. Atsumi, Chem. Lett., 187 (1974).
T. Cohen and R. E. Gapinski, Tetrahedron Lett., No. 45, 4318 (1978).
R. P. Hatch and S. M. Weinreb, J. Org. Chem., 42, 3960 (1977).
S. Masamune, S. Kamata, J. Diakur, I. Sugihara, and G. S. Bates, Can. J. Chem., 53, 3693 (1975).
H. J. Gais and T. Lied, Angew. Chem., Int. Ed., 17, 267 (1978).
S. Ohta and M. Okamoto, Tetrahedron Lett., 22, 3245 (1981).
P. A. Grieco, Y. Yokoyama, and E. Williams, J. Org. Chem., 43, 1283 (1978).
T. Mukaiyama, Synth. Commun., 2, 243 (1972).
A. é. Sausin', V. K. Lusis, B. S. Chekavichus, and G. Ya. Dubur, Khim. Geterotsikl. Soedin., No. 8, 1072 (1982).
B. S. Chekavichus, A. S. Sausin, and G. Ya. Dubur, Khim. Geterotsikl. Soedin., No. 8, 1072 (1982).
Ya. R. Uldrikis, G. Ya. Dubur, I. V. Dipan, and B. S. Chekavichus, Khim. Geterotsikl. Soedin., No. 9, 1230 (1975).
P. J. Brignell, U. Eisner, and P. G. Farrell, J. Chem. Soc., Perkin Trans. 2, No. 11, 1083 (1966).
V. K. Lusis and G. Ya. Dubur, Khim. Geterotsikl. Soedin., No. 8, 1067 (1982).
S. Oae, Chemistry of Organic Sulfur Compounds [in Russian], Khimiya, Moscow (1975), p. 139.
T. Chennat and U. Eisner, J. Chem. Soc., Perkin Trans 1, No. 10, 926 (1975).
B. A. Vigante, Ya. Ya. Ozols, B. S. Chekavichus, and G. Ya. Dubur, Khim. Geterotsikl. Soedin., No. 9, 1232 (1988).
Author information
Authors and Affiliations
Additional information
Translated from Khimiya Geterotsiklicheskikh Soedinenii, No. 7, pp. 953–958, July, 1991.
Rights and permissions
About this article
Cite this article
Vigante, B.A., Ozols, Y.Y. & Dubur, G.Y. 1,4-Dihydropyridine-3,5-dicarbothionic acid S-esters. Chem Heterocycl Compd 27, 762–767 (1991). https://doi.org/10.1007/BF00476209
Received:
Revised:
Issue Date:
DOI: https://doi.org/10.1007/BF00476209