Abstract
Bisuracil sulfolane derivatives have been synthesized using the silyl method of nucleoside synthesis in the presence of SnCl4. The necessary starting materials were 5-hydroxy-6-methyluraciI (prepared by oxidation of 6-methyluracil with ammonium persulfate in aqueous medium) and trans-3,4-diacetoxysulfolane (prepared from trans-3,4-dihydroxysulfolane). The structures of the bisuracil sulfolane derivatives were established based on their spectral data and elemental analysis.
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Translated from Khimiya Geterotsiklicheskikh Soedinenii, No. 9, pp. 1235–1237, September, 1990.
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Tolstikov, G.A., Sharipova, F.V., Baltina, L.A. et al. Synthesis of bisuracil sulfolane derivatives. Chem Heterocycl Compd 26, 1030–1032 (1990). https://doi.org/10.1007/BF00472487
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DOI: https://doi.org/10.1007/BF00472487