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Stereoisomers of 2-methyl-1-thiadecalin

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Chemistry of Heterocyclic Compounds Aims and scope

Abstract

A mixture of the geometrical isomers of 2-methyl-1-thiadecalin has been separated by a combination of adsorption column chromatography and preparative gas-liquid chromatography. The configuration of each isomer has been established by mass spectrometry and PMR spectrometry with the application of the Auwers-Skita rule.

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Authors and Affiliations

  1. Institute of Petrochemical Synthesis, Academy of Sciences of the USSR, Moscow

    E. N. Karaulova, L. M. Petrova, G. D. Gal'pern, A. Yu. Koshevnik, E. S. Brodskii, I. M. Lukashenko & F. V. Kozlova

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  1. E. N. Karaulova
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  2. L. M. Petrova
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  3. G. D. Gal'pern
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  4. A. Yu. Koshevnik
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  5. E. S. Brodskii
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  6. I. M. Lukashenko
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  7. F. V. Kozlova
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Translated from Khimiya Geterotsiklicheskikh Soedinenii, No. 7, pp. 913–917, July, 1973.

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Karaulova, E.N., Petrova, L.M., Gal'pern, G.D. et al. Stereoisomers of 2-methyl-1-thiadecalin. Chem Heterocycl Compd 9, 841–844 (1973). https://doi.org/10.1007/BF00471563

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  • DOI: https://doi.org/10.1007/BF00471563

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