Skip to main content
Log in

Yield stress behaviour of metal injection moulding suspensions at elevated temperatures

  • Papers
  • Published:
Journal of Materials Science Aims and scope Submit manuscript

Abstract

Yield behaviour of metal injection moulding (MIM) feedstocks was studied using a cone and plate controlled stress rheometer. Four feedstocks consisting of 58 vol % carbonyl iron (with 2 wt % nickel) in different ethylene vinyl acetate (EVA):beeswax ratio binder systems were studied at six temperatures ranging from 130 to 180‡C. The yield stress was found by extrapolating to zero shear rate of the measured data obtained using a controlled stress rheometer over low shear rate regime. The yield stress, ρy, was found to increase with decreasing temperature. An Arrhenius equation was used to relate the dependence of yield stress on temperature and the corresponding activation energy for yield, E y, can be determined. For a given temperature, feedstocks with higher EVA content exhibited higher Τy and E y. Moreover, the effect of temperature on yield stress was found to be greater for feedstocks with higher EVA content.

This is a preview of subscription content, log in via an institution to check access.

Access this article

Price excludes VAT (USA)
Tax calculation will be finalised during checkout.

Instant access to the full article PDF.

Institutional subscriptions

Similar content being viewed by others

References

  1. R. A. PETT, V. D. N. RAO and S. B. A. QADERI, US Patent 4 158 689 (1979).

  2. R. D. RIVERS, US Patent 4 113 480 (1978).

  3. R. E. WIECH Jr, US Patent 4 197 118 (1980).

  4. Idem, US Patent 4 415 528 (1983).

  5. K. P. JOHNSON, US Patent 4 765 950 (1988).

  6. R. L. BILLIET, US Patent 4 795 598 (1989).

  7. Y. KIYOTA, US Patent 4 867 943 (1989).

  8. T. NAGAI, H. YAMANASHI and H. HACHIMORI, US Patent 4 898 902 (1990).

  9. M. NAKANISHI and T. MIHO, US Patent 4 968 739 (1990).

  10. C. A. SUNDBACK, B. E. NOVICH, A. E. KARAS and R. W. ADAMS, US Patent 5 047 182 (1991).

  11. R. M. German, “Powder Injection Molding” (Metal Powders Industries Federation, NJ, 1990) p. 176.

    Google Scholar 

  12. M. J. Edirisinghe and J. R. G. Evans, J. Mater. Sci. 22 (1987) 269.

    Article  CAS  Google Scholar 

  13. R. M. German, “Powder Injection Molding” (Metal Powders Industries Federation, NJ, 1990) p. 160.

    Google Scholar 

  14. Idem, ibid. p. 158, 173, 231.

    Google Scholar 

  15. B.O. RHEE, PhD thesis, Renssalaer Polytechnic Institute (1992).

  16. E. Windhab, “Proceedings of the Tenth International Congress on Rheology, Sydney”, edited by P. H. T. Uhlherr (Society of Rheology, Sydney, 1988) p. 372.

    Google Scholar 

  17. Q. D. Nguyen and D. V. Boger, Ann. Rev. Fluid Mech. 24 (1992) 47.

    Article  Google Scholar 

  18. J. P. Harnett and R. Y. Z. Hu, J. Rheol. 33(4) (1989) 671.

    Article  Google Scholar 

  19. D. D. Kee and C. F. Chan Man Fong, J. Rheol. 37(4) (1993) 775.

    Article  Google Scholar 

  20. D. D. Kee and C. J. Durning, in “Polymer Rheology and Processing”, edited by A. A. Collyer and L. A. Utracki (Elsevier Science Publishers, England, 1990) p. 177.

    Google Scholar 

  21. Q. D. Nguyen and D. V. Boger, J. Rheol. 29(3) (1985) 335.

    Article  Google Scholar 

  22. Idem, ibid. 27(4) (1983) 321.

    Article  Google Scholar 

  23. D. M. Kalyon, P. Yaras, B. Aral and U. Yilmazer, ibid. 37(1) (1993) 35.

    Article  CAS  Google Scholar 

  24. L. Bohlin, in “Proceedings of the Tenth International Congress on Rheology, Sydney”, edited by P. H. T. Uhlherr (Society of Rheology, Sydney, 1988) p. 191.

    Google Scholar 

  25. P. J. Hansen and M. C. Williams, Polym. Eng. Sci. 27(8) (1987) 586.

    Article  CAS  Google Scholar 

  26. A. Magnin and J. M. Piau, J. Non-Newtonian Fluid Mech. 36 (1990) 85.

    Article  CAS  Google Scholar 

  27. Idem, ibid. 23 (1987) 91.

    Article  CAS  Google Scholar 

  28. A. S. Yoshimura, R. K. Prud'homme and H. M. Princen, J. Rheol. 31(8) (1987) 699.

    Article  CAS  Google Scholar 

  29. E. C. Bingham, “Fluidity and Plasticity” (McGraw-Hill, New York, 1922).

    Google Scholar 

  30. W. H. Herschel and R. Bulkley, Proc. ASTM 26 (1926) 621.

    Google Scholar 

  31. W. Casson, in “Rheology of Dispersed Systems”, edited by C. C. Mill (Pergamon, London, 1959) p. 84.

    Google Scholar 

  32. M. Henderson, IEEE Electrical Insulation Mag. 9(1) (1993) 30.

    Article  Google Scholar 

  33. B. O. Rhee and C. I. Chung, “Proceedings of the Fourth APP Annual Meeting” (Metal Powders Industries Fed., NJ, 1990).

    Google Scholar 

  34. C. I. Chung, M. Y. Cao and B. O. Rhee, ibid.“.

    Google Scholar 

  35. “Instruction Manual for the Carri-Med CSL Controlled Stress Rheometer”, edited by CarriMed Ltd, UK.

  36. D. M. Husband, N. Aksel and W. Gieissle, J. Rheol. 37(2) (1993) 215.

    Article  CAS  Google Scholar 

  37. N. Ohl and W. Gleissle, ibid. 37(2) (1993) 381.

    Article  CAS  Google Scholar 

  38. A. Y. Malkin, Adv. Polym. Sci. 96 (1990) 70.

    Google Scholar 

  39. H. Tanaka and J. L. White, J. Non-Newtonian Fluid Mech. 7 (1980) 333.

    Article  CAS  Google Scholar 

  40. Idem, Polym. Eng. Sci. 20(14) (1980) 949.

    Article  CAS  Google Scholar 

Download references

Author information

Authors and Affiliations

Authors

Rights and permissions

Reprints and permissions

About this article

Cite this article

Foong, M.L., Tam, K.C. & Loh, N.H. Yield stress behaviour of metal injection moulding suspensions at elevated temperatures. JOURNAL OF MATERIALS SCIENCE 30, 3625–3632 (1995). https://doi.org/10.1007/BF00351876

Download citation

  • Received:

  • Accepted:

  • Published:

  • Issue Date:

  • DOI: https://doi.org/10.1007/BF00351876

Keywords

Navigation