Summary
In the proposed method excess of Soxhlet reagent is added to the sugar standard solutions and the unknown samples; the reduction of Cu(II) to Cu2O is taking place by heating at constant temperature for a specified time. Unreduced copper in the supernatant solution or reduced copper in the Cu2O precipitate is determined by PSA. The method offers the following advantages for the determination of reducing sugars in soft drinks, wines, spirituous liquors, honey, marmalades etc.: 1) high sensitivity, due to the PSA-technique; 2) applicability to coloured and turbid samples where the official methods cannot be applied without preceding treatment of the sample; 3) good agreement with standard methods for the assay of sugars.
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References
Kolthoff MI, Belcher R (1957) Volumetric analysis, vol III. Interscience, New York
Horwitz W (ed) (1975) Official methods of analysis of the association of official analytical chemists, 12th edn. AOAC, Washington, D.C. 20044
Papastathopoulos DS, Nikolelis DP, Hadjiioannou TP (1977) Analyst 102:852–857
Gritzapis PC, Timotheou-Potamia M (1977) Anal Chim Acta 218:37–46
Efstathiou CE, Hadjiioannou TP (1977) Anal Chim Acta 89:55–63
Maquieira A, Luque de Castro MD, Valcárcel M (1987) Analyst 112:1569–1572
Jagner D (1978) Anal Chem 50:1924–1929
Jagner D, Graneli A (1976) Anal Chim Acta 83:19–26
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Nanos, C.G., Karayannis, M.I. Assay of reducing sugars in beverages, wines, honey and marmalades using potentiometric stripping analysis (PSA). Fresenius J Anal Chem 340, 253–257 (1991). https://doi.org/10.1007/BF00321779
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DOI: https://doi.org/10.1007/BF00321779