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Flow-injection determination of HMF in honey by the Winkler method

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Summary

A new method for the semiautomatic determination of 5-hydroxymethylfurfural (HMF) by photometric flow injection analysis on the basis of the Winkler's reaction is proposed. The derivative FIA-gram signals were also obtained and detection limit was decreased. The linear range of determination is 2.3–98 μg·ml−1. The presence of sugars is well tolerated. The proposed method can be employed to determine HMF in honey samples with a sampling frequency of 35 h−1.

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Authors and Affiliations

  1. Department of Analytical Chemistry, University of Extremadura, E-06071, Badajoz, Spain

    F. Salinas & A. Espinosa Mansilla

  2. Department of Chemistry, University of Castilla-La Mancha, E-13071, Ciudad Real, Spain

    A. Espinosa Mansilla & J. J. Berzas Nevado

Authors
  1. F. Salinas
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  2. A. Espinosa Mansilla
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  3. J. J. Berzas Nevado
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Salinas, F., Mansilla, A.E. & Berzas Nevado, J.J. Flow-injection determination of HMF in honey by the Winkler method. Fresenius J Anal Chem 340, 250–252 (1991). https://doi.org/10.1007/BF00321778

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  • DOI: https://doi.org/10.1007/BF00321778

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