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Interactions between HA/GO/epoxy resin nanocomposites: optimization, modeling and mechanical performance using central composite design and genetic algorithm

  • A. DadrasiEmail author
  • S. Fooladpanjeh
  • A. Alavi Gharahbagh
Technical Paper
  • 45 Downloads

Abstract

This study is focused on the role of hydroxyapatite (HA) nanoparticles and graphene oxide (GO) nanoplates on the flexural and compression properties of epoxy-based hybrid nanocomposites. In the first step, epoxy-based hybrid nanocomposites were reinforced by different HA nanoparticles and GO nanoplates up to 7 wt% and 0.5 wt%, respectively. Filler’s weight fractions that used as design parameters have been achieved by central composite design method in Minitab software. The experimental results showed different combinations of HA- and GO-enhanced mentioned mechanical properties in various states. In the second step, a statistical modeling has been done by response surface method (RSM), artificial neural network (ANN) and decision tree methods. Modeling results showed that ANN and decision tree methods have the best fitness. Finally, the mechanical properties are optimized by genetic algorithm. The optimum values are 21.54 MPa for flexural strength in 5.17 wt% HA and 0.38 wt% Go and 25.7 GPa for flexural modulus in 2.73 wt% HA and 0.195 wt% GO. Also, the optimum results for compression strength are 23.95 MPa in 7 wt% HA and 0.289 wt% GO, and also 690.5 MPa for compression modulus in 6.89 wt% HA and 0.007 wt% GO. Effective mechanisms of fillers have been analyzed by SEM and observed that debonding, crack path deflection, plastic void growth and pullout were dominant.

Keywords

Mechanical properties Hydroxyapatite Graphene oxide Central composite design Artificial neural network Genetic algorithm 

References

  1. 1.
    Chen X, Liu L, Pan F, Mao J, Xu X, Yan T (2015) Microstructure, electromagnetic shielding effectiveness and mechanical properties of Mg–Zn–Cu–Zr alloys. Mater Sci Eng B 197:67–74CrossRefGoogle Scholar
  2. 2.
    Rai A, Subramanian N, Chattopadhyay A (2017) Investigation of damage mechanisms in CNT nanocomposites using multiscale analysis. Int J Solids Struct 120:115–124CrossRefGoogle Scholar
  3. 3.
    Feng Q, Yang J, Yu Y, Tian F, Zhang B, Feng M, Wang S (2017) The ionic conductivity, mechanical performance and morphology of two phase structural electrolytes based on polyethylene glycol, epoxy resin and nano-silica. Mater Sci Eng B 219:37–44CrossRefGoogle Scholar
  4. 4.
    Raju T, Ding YM, Yang L, Paula M, Yang WM, Tibor C, Sabu T (2008) Miscibility, morphology, thermal, and mechanical properties of a DGEBA based epoxy resin toughened with a liquid rubber. Polymer 49:278–294CrossRefGoogle Scholar
  5. 5.
    Xiao J, Shu DW, Wang XJ (2014) Effect of strain rate and temperature on the mechanical behavior of magnesium nanocomposites. Int J Mech Sci 89:381–390CrossRefGoogle Scholar
  6. 6.
    Feli S, Jafari SS (2017) Analytical modeling for perforation of foam-composite sandwich panels under high-velocity impact. J Braz Soc Mech Sci 39:401–412CrossRefGoogle Scholar
  7. 7.
    Krumova M, Klingshirn C, Haupert F, Friedrich K (2001) Microhardness studies on functionally graded polymer composites. Compos Sci Technol 61:557–563CrossRefGoogle Scholar
  8. 8.
    Braga RA, Magalhaes PAA (2015) Analysis of the mechanical and thermal properties of jute and glass fiber as reinforcement epoxy hybrid composites. Mater Sci Eng C 56:269–273CrossRefGoogle Scholar
  9. 9.
    Baradaran S, Moghaddam E, Basirun WJ, Mehrali M, Sookhakian M, Hamdi M, Moghaddam MRN, Alias N (2014) Mechanical properties and biomedical applications of a nanotube hydroxyapatite-reduced graphene oxide composite. Carbon 69:32–45CrossRefGoogle Scholar
  10. 10.
    Zhang S, Wang YS, Zeng XT, Khor KA, Weng W, Sun DE (2008) Evaluation of a adhesion strength and toughness of fluoridated hydroxyapatite coatings. Thin Solid Films 516:5162–5167CrossRefGoogle Scholar
  11. 11.
    Mebaraki Y, Rechak S, Marc D, Maslouhi A (2014) Effect of interfacial powder on mechanical properties of composites under dynamic tests. J Braz Soc Mech Sci 36:939–949CrossRefGoogle Scholar
  12. 12.
    Stankovic VM, Erakovic S, Jankovic A, Sekulic MV, Mitric M, Jung YC, Park SJ, Phee KY (2015) Electrochemical synthesis of nanosized hydroxyapatite/graphene composite powder. Carbon Lett 16:233–240CrossRefGoogle Scholar
  13. 13.
    Zhao JL, Fu T, Han Y, Xu KW (2003) Reinforcing hydroxyapatite/thermosetting epoxy composite with 3-D carbon fiber fabric through RTM processing. Mater Lett 58:163–168CrossRefGoogle Scholar
  14. 14.
    Li J, Lu XL, Zheng YF (2008) Effect of surface modified hydroxyapatite on the tensile property improvement of HA/PLA composite. Appl Surf Sci 255:494–497CrossRefGoogle Scholar
  15. 15.
    Zebarjad M, Sajjadi SA, Sdrabadi TE, Yaghmaei A, Naderi B (2011) A study on mechanical properties of PMMA/hydroxyapatite nanocomposite. Engineering 3:795–801CrossRefGoogle Scholar
  16. 16.
    Rose LRF (1987) Toughening due to crack-front interaction with a second-phase dispersion. Mech Mater 6:11–15CrossRefGoogle Scholar
  17. 17.
    Faber KT, Evans AG (1983) Crack deflection processes-II, experiment. Acta Metallurgica 31:577–584CrossRefGoogle Scholar
  18. 18.
    Maazouz A, Sautereau H, Gerard JF (1993) Hybrid-particulate composites based on an epoxy matrix, a reactive rubber, and glass beads: morphology, viscoelastic, and mechanical properties. J Appl Polym Sci 50:615–626CrossRefGoogle Scholar
  19. 19.
    Osorio AG, Dos Santos LA, Bergmann CP (2011) Evaluation of the mechanical properties and microstructure of hydroxyapatite reinforced with carbon nanotubes. Rev Adv Mater Sci 27:58–63Google Scholar
  20. 20.
    Huang G, Wang S, Song P, Wu C, Chen S, Wang X (2014) Combination effect of carbon nanotubes with graphene on intumescent flame-retardant polypropylene nanocomposites. Compos Part A 59:18–25CrossRefGoogle Scholar
  21. 21.
    Akao M, Aoki H, Kato K (1981) Mechanical properties of sintered hydroxyapatite for prosthetic applications. J Mater Sci 16:809–812CrossRefGoogle Scholar
  22. 22.
    Harichandran R, Selvakumar N (2018) Microstructure and mechanical characterization of (B4C + h-BN)/Al hybrid nanocomposites processed by ultrasound assisted casting. Int J Mech Sci 144:814–826CrossRefGoogle Scholar
  23. 23.
    Martin RB, Chapman MW, Sharkey NA, Zissimos SL, Bay B, Shors EG (1993) Bone ingrowth and mechanical properties of coralline hydroxyapatite 1 yr after implantation. Biomaterials 14:341–348CrossRefGoogle Scholar
  24. 24.
    Paliwal B, Cherkaoui M (2012) Estimation of anisotropic elastic properties of nanocomposites using atomistic-continuum interphase model. Int J Solids Struct 49(18):2424–2438CrossRefGoogle Scholar
  25. 25.
    Nadeem S, Hina S (2017) Exploration of single wall carbon nanotubes for the peristaltic motion in a curved channel with variable viscosity. J Braz Soc Mech Sci 39:117–125CrossRefGoogle Scholar
  26. 26.
    Xu Y, Sheng K, Li Ch, Shi G (2010) Self-assembled graphene hydrogel via a one-step hydrothermal process. ACS Nano 4(7):4324–4330CrossRefGoogle Scholar
  27. 27.
    Shenghua L, Yujuan M, Chaochao Q, Sun T, Jingjing T, Qingfang Z (2013) Effect of graphene oxide nanosheets of microstructure and mechanical properties of cement composites. Constr Build Mater 49:121–127CrossRefGoogle Scholar
  28. 28.
    Fereidoon A, Memarian S, Albooyeh A, Tarahomi S (2014) Influence of mesoporous silica and hydroxyapatite nanoparticles on the mechanical and morphological properties of polypropylene. Mater Des 57:201–210CrossRefGoogle Scholar
  29. 29.
    Hastie TJ, Tibshirani RJ, Friedman JH (2009) The elements of statistical learning: data mining inference and prediction, 2nd edn. Springer, BerlinCrossRefGoogle Scholar
  30. 30.
    Ciresan D (2012) Multi-column deep neural network for traffic sign classification. Neural Netw 32:333–338CrossRefGoogle Scholar
  31. 31.
    Goldberg DE (1989) Genetic algorithms in search, optimization, and machine learning. Addison-Wesley, ReadingzbMATHGoogle Scholar
  32. 32.
    Haupt RL, Haupt SE (1998) Practical genetic algorithms. Wiley, New YorkzbMATHGoogle Scholar
  33. 33.
    Haupt RL, Haupt SE (2004) Practical genetic algorithms, 2nd edn. Wiley, New YorkzbMATHGoogle Scholar
  34. 34.
    Balguri PK, Samuel DGH, Mahadevan SM, Thumu U (2017) Effect of thiolated-silver quantum clusters on flexural properties of epoxy polymer. Mater Today: Proc 4:4108–4115CrossRefGoogle Scholar
  35. 35.
    Shokrieh MM, Esmkhani M, Haghighatkhah AR, Zhao Z (2014) Flexural fatigue behavior of synthesized graphene/carbon-nanofiber/epoxy hybrid nanocomposites. Mater Des 62:401–408CrossRefGoogle Scholar
  36. 36.
    Rafiee MA, Rafiee J, Wang Z, Song H, Yu ZZ, Koratkar N (2009) Enhanced mechanical properties of nanocomposites at low graphene. ACS Nano 3(12):3884–3890CrossRefGoogle Scholar
  37. 37.
    Liu HY, Wang GT, Mai YW, Zeng Y (2011) On fracture toughness of nano-particle modified epoxy. Compos Part B 42:2170–2175CrossRefGoogle Scholar
  38. 38.
    Liu HY, Wang G, Mai YW (2012) Cyclic fatigue crack propagation of nanoparticle modified epoxy. Compos Sci Technol 72:1530–1538CrossRefGoogle Scholar
  39. 39.
    Li Z, Guo Q, Li Z, Fan G, Xiong DB, Su Y, Zhang J, Zhang D (2015) Enhanced mechanical properties of graphene (reduced graphene oxide)/aluminum composites with a bioinspired nanolaminated structure. Nano Lett 15:8077–8083CrossRefGoogle Scholar
  40. 40.
    Cheng Y, Zhang Y, Wan T, Yin T, Wang J (2017) Mechanical properties and toughening mechanisms of graphene platelets reinforced Al2O3/TiC composite ceramic tool materials by microwave sintering. Mater Sci Eng A 680:190–196CrossRefGoogle Scholar
  41. 41.
    Palmeri MJ, Putz KW, Brinson LC (2010) Toughening of high performance epoxies via nanofiber sacrificial bond mechanisms. ACS Nano 4:4256–4264CrossRefGoogle Scholar
  42. 42.
    Wang X, Jin J, Song M (2013) An investigation of the mechanism of graphene toughening epoxy. Carbon 65:324–333CrossRefGoogle Scholar
  43. 43.
    Ritchie R (1988) Mechanisms of fatigue crack propagation in metals, ceramics and composites: role of crack tip shielding. Mater Sci Eng A 103:15–28CrossRefGoogle Scholar
  44. 44.
    Williams JG (2010) Particle toughening of polymers by plastic void growth. Compos Sci Technol 70:885–891CrossRefGoogle Scholar
  45. 45.
    Quaresimin M, Salviato M, Zappalorto M (2015) Toughening mechanisms in nanoparticle polymer composites: experimental evidences and modeling. In: Toughening mechanisms in composite materials, pp 113–133Google Scholar
  46. 46.
    Shokrieh MM, Zeinedini A (2016) Effect of CNTs debonding on mode I fracture toughness of polymeric nanocomposites. Mater Des 101:56–65CrossRefGoogle Scholar
  47. 47.
    Gojny FH, Wichmann MHG, Fiedler B, Schulte K (2005) Influence of different carbon nanotubes on the mechanical properties of epoxy matrix composites—a comparative study. Compos Sci Technol 65:2300–2313CrossRefGoogle Scholar
  48. 48.
    Hao Y, Hao H (2017) Pull-out behaviour of spiral-shaped steel fibers from normal-strength concrete matrix. Constr Build Mater 139:34–44CrossRefGoogle Scholar
  49. 49.
    Wille K, Naaman A (2012) Pullout behavior of high-strength steel fibers embedded in ultra-high-performance concrete. ACI Mater J 109(4):479–488Google Scholar
  50. 50.
    Buratti N, Mazzotti C, Savoia M (2011) Post-cracking behaviour of steel and macrosynthetic fibre-reinforced concretes. Constr Build Mater 25:2713–2722CrossRefGoogle Scholar
  51. 51.
    Babafemi AJ, Boshoff WP (2015) Tensile creep of macro-synthetic fibre reinforced concrete (MSFRC) under uni-axial tensile loading. Cem Concr Compos 55:62–69CrossRefGoogle Scholar
  52. 52.
    Babafemi AJ, Boshoff WP (2017) Pull-out response of macro synthetic fiber from concrete matrix: effect of loading rate and embedment length. Constr Build Mater 135:590–599CrossRefGoogle Scholar
  53. 53.
    Carlos VO, Coelho LAF (2016) Reinforcement and toughening mechanisms in polymer nanocomposites—reinforcement effectiveness and nanoclay nanocomposites. Mater Chem Phys 169:179–185CrossRefGoogle Scholar
  54. 54.
    Opelt CV, Becker D, Lepienski CM, Coelho LAF (2015) Reinforcement and toughening mechanisms in polymer nanocomposites—carbon nanotubes and aluminum oxide. Compos B Eng 75:119–126CrossRefGoogle Scholar
  55. 55.
    Ahmad I, Cao HZ, Chen HH, Zhao HY, Kennedy A, Zhu YQ (2010) Carbon nanotube toughened aluminium oxide nanocomposite. J Eur Ceram Soc 30:865–873CrossRefGoogle Scholar
  56. 56.
    Chang Q, Chen DL, Ru HQ, Yue XY, Yu L, Zhang CP (2010) Toughening mechanisms in iron-containing hydroxyapatite/titanium composites. Biomaterials 31(14):93–1501CrossRefGoogle Scholar

Copyright information

© The Brazilian Society of Mechanical Sciences and Engineering 2019

Authors and Affiliations

  1. 1.Department of Mechanical Engineering, Shahrood BranchIslamic Azad UniversityShahroodIran
  2. 2.Department of Electronic and Computer Engineering, Shahrood BranchIslamic Azad UniversityShahroodIran

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