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Chemical Research in Chinese Universities

, Volume 35, Issue 4, pp 560–563 | Cite as

Solvothermal Syntheses and Characterization of Three One-dimension Cadmium Selenidoarsenates [Ni(1,2-dap)3][As2CdSe4], [Zn(1,2-dap)3][As2CdSe4] and [Ni(en)3][As2CdSe4]

  • Cuixia Du
  • Juan Chen
  • Menghe BaiyinEmail author
Article
  • 31 Downloads

Abstract

Three new cadmium selenidoarsenates, [Ni(1,2-dap)3][As2CdSe4](1)(1,2-dap=1,2-diaminopropane), [Zn(1,2-dap)3][As2CdSe4](2) and [Ni(en)3][As2CdSe4](3)(en=ethylenediamine), were synthesized under solvothermal conditions. And they are isostructural and monoclinic crystalls. As seen from their structures, they exhibited one-dimensional(1D) chains composed of [As2CdSe4]2- anions and [TM(amine)3]2+(TM=Ni, Zn; amine=1,2-dap, en) cations. Their absorption edges are 2.32, 1.84 and 2.38 e V, and they show the properties of the semiconductor. These compounds were also characterized by means of single-crystal X-ray diffraction(XRD), powder X-ray diffraction (PXRD), solid-state optical absorption spectrometry, and so on.

Keywords

Solvothermal synthesis Selenidoarsenate Cadmium 

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Supplementary material

40242_2019_9011_MOESM1_ESM.pdf (231 kb)
Solvothermal Syntheses and Characterization of Three One-Dimension Cadmium Selenidoarsenates [Ni(1,2-dap)3][As2CdSe4], [Zn(1,2-dap)3][As2CdSe4] and [Ni(en)3][As2CdSe4]

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Copyright information

© Jilin University, The Editorial Department of Chemical Research in Chinese Universities and Springer-Verlag GmbH 2019

Authors and Affiliations

  1. 1.College of Chemistry & Environmental ScienceInner Mongolia Normal UniversityHohhotP. R. China

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