Advertisement

Magnetic nano-carbon core shell as potent mixed hemimicelle solid phase extraction strategy for determination of acrylamide from potato chips coupled by high-performance liquid chromatography

  • Arezou Taghvimi
  • Samin Hamidi
  • Yousef Javadzadeh
  • Siavoush Dastmalchi
  • Mahnaz TabibiazarEmail author
Original Paper
  • 8 Downloads

Abstract

Magnetic nano-carbon core shell was applied as mixed hemimicelle magnetic solid phase extraction adsorbent to introduce a novel sample preparation method for determination of acrylamide from potato chips. Acrylamide is identified as neurotoxic, a probable human carcinogen (group 2A) compound. Effective extraction parameters such as type and amount of extracting solvent, type and amount of adsorbent, time of extraction and desorption, the effect of pH, time of ionic liquid loading on the adsorbent and stirring rate (rpm) were studied and optimized. Under optimized extraction conditions, a good linearity was observed in the concentration range of 100–1500 ng/g. Limit of detection was observed as 30 ng/g. Application of the proposed method was surveyed by analysis of some potato chips brands available in the local supermarkets. The satisfactory results with the recovery of 95.58% revealed that the proposed method could be applied in food analysis laboratories.

Keywords

Magnetic solid phase extraction Mixed hemimicelle Magnetic nano-carbon core shell Potato chips Acrylamide HPLC–UV 

Abbreviations

MNC

Magnetic nano-carbon

LLE

Liquid–liquid extraction

MNPs

Magnetic nanoparticles

NPs

Nanoparticles

SPME

Solid phase micro-extraction

IL

Ionic liquid

MSPE

Magnetic solid phase extraction

DLLE

Dispersive liquid–liquid micro-extraction

EFSA

European food safety authority

IL-MNC

Ionic liquid magnetic nano-carbon

Notes

Acknowledgement

The authors sincerely appreciate Biotechnology Research Centre and Faculty of Nutrition and Food Science of Tabriz University of Medical Sciences for supporting the project.

Funding

This research did not receive any specific grant from funding agencies in the public, commercial or not-for-profit sectors. Conflict of interest: All the authors declare that there is no conflict of interest.

Compliance with ethical standards

Ethical approval

This article does not contain any studies with human participants or animals performed by any of the authors.

Informed consent

Not applicable.

References

  1. 1.
    A.P. Arisseto, M.C. de Figueiredo Toledo, Y. Govaert, J. van Loco, S. Fraselle, J.-M. Degroodt, Food Anal Method. 1, 49–55 (2008)CrossRefGoogle Scholar
  2. 2.
    H. Zhao, B. Dai, L. Xu, X. Wang, X. Qiao, Z. Xu, J. Sci. Food Agric. 94, 1787–1793 (2014)CrossRefGoogle Scholar
  3. 3.
    H. Ayvaz, L.E. Rodriguez-Saona, Food Chem. 174, 154–162 (2015)CrossRefGoogle Scholar
  4. 4.
    V. Gökmen, H.Z. Şenyuva, J. Acar, K. Sarıoğlu, J. Chromatogr. A 1088, 193–199 (2005)CrossRefGoogle Scholar
  5. 5.
    M. Arabi, A. Ostovan, M. Ghaedi, M.K. Purkait, Talanta 154, 526–532 (2016)CrossRefGoogle Scholar
  6. 6.
    E. Norouzi, M. Kamankesh, A. Mohammadi, A. Attaran, J. Cereal Sci. 79, 1–5 (2018)CrossRefGoogle Scholar
  7. 7.
    Y. Zhu, G. Li, Y. Duan, S. Chen, C. Zhang, Y. Li, Food Chem. 109, 899–908 (2008)CrossRefGoogle Scholar
  8. 8.
    Y. Zhang, Y. Ren, H. Zhao, Y. Zhang, Anal. Chim. Acta 584, 322–332 (2007)CrossRefGoogle Scholar
  9. 9.
    L. Xu, X. Qiao, Y. Ma, X. Zhang, Z. Xu, Food Anal Method. 6, 838–844 (2013)CrossRefGoogle Scholar
  10. 10.
    D. Taeymans, J. Wood, P. Ashby, I. Blank, A. Studer, R.H. Stadler, P. Gonde, P. Eijck, S. Lalljie, H. Lingnert, Crit. Rev. Food Sci. Nutr. 44, 323–347 (2004)CrossRefGoogle Scholar
  11. 11.
    S.E.K. Tekkeli, C. Önal, A. Önal, Food Anal Method. 5, 29–39 (2012)CrossRefGoogle Scholar
  12. 12.
    I.G. Casella, M. Pierri, M. Contursi, J. Chromatogr. A 1107, 198–203 (2006)CrossRefGoogle Scholar
  13. 13.
    J.R. Pedersen, J.O. Olsson, Analyst 128, 332–334 (2003)CrossRefGoogle Scholar
  14. 14.
    S.-L. Xie, K. Wang, R.-Z. Zhu, X.-W. Zhu, W.-Z. Wei, Mendeleev Commun. 19, 344–345 (2009)CrossRefGoogle Scholar
  15. 15.
    M. Rezaee, Y. Assadi, M.-R.M. Hosseini, E. Aghaee, F. Ahmadi, S. Berijani, J. Chromatogr. A 1116, 1–9 (2006)CrossRefGoogle Scholar
  16. 16.
    L. Xie, R. Jiang, F. Zhu, H. Liu, G. Ouyang, Anal. Bioanal. Chem. 406, 377–399 (2014)CrossRefGoogle Scholar
  17. 17.
    P.-C. Lin, M.-C. Tseng, A.-K. Su, Y.-J. Chen, C.-C. Lin, Anal. Chem. 79, 3401–3408 (2007)CrossRefGoogle Scholar
  18. 18.
    B.N. Vanderpuije, G. Han, V.M. Rotello, R.W. Vachet, Anal. Chem. 78, 5491–5496 (2006)CrossRefGoogle Scholar
  19. 19.
    A. Jouyban, S. Hamidi, J. Sep. Sci. 40, 3318–3326 (2017)CrossRefGoogle Scholar
  20. 20.
    S. Chikazumi, S. Taketomi, M. Ukita, M. Mizukami, H. Miyajima, M. Setogawa, Y. Kurihara, J. Magn. Magn. Mater. 65, 245–251 (1987)CrossRefGoogle Scholar
  21. 21.
    A.H. Lu, W. Schmidt, N. Matoussevitch, H. Bönnemann, B. Spliethoff, B. Tesche, E. Bill, W. Kiefer, F. Schüth, Angew. Chem. 116, 4403–4406 (2004)CrossRefGoogle Scholar
  22. 22.
    Z. Li, L. Wei, M. Gao, H. Lei, Adv. Mater. 17, 1001–1005 (2005)CrossRefGoogle Scholar
  23. 23.
    M. Šafařı́ková, I. Šafařı́k, J. Magn. Magn. Mater. 194, 108–112 (1999)CrossRefGoogle Scholar
  24. 24.
    H. Heidari, H. Razmi, Talanta 99, 13–21 (2012)CrossRefGoogle Scholar
  25. 25.
    A. Taghvimi, H. Hamishehkar, M. Ebrahimi, J. Chromatogr. B 1009, 66–72 (2016)CrossRefGoogle Scholar
  26. 26.
    H. He, D. Yuan, Z. Gao, D. Xiao, H. He, H. Dai, J. Peng, N. Li, J. Chromatogr. A 1324, 78–85 (2014)CrossRefGoogle Scholar
  27. 27.
    J. Wu, H. Zhao, D. Xiao, P.-H. Chuong, J. He, H. He, J. Chromatogr. A 1454, 1–8 (2016)CrossRefGoogle Scholar
  28. 28.
    A. Taghvimi, S. Hamidi, Y. Javadzadeh, J. Sep. Sci. 42, 582–590 (2019)CrossRefGoogle Scholar
  29. 29.
    A. Taghvimi, H. Hamishehkar, J. Chromatogr. B 1041, 113–119 (2017)CrossRefGoogle Scholar
  30. 30.
    M. Zokaei, A.-S. Abedi, M. Kamankesh, S. Shojaee-Aliababadi, A. Mohammadi, Food Chem. 234, 55–61 (2017)CrossRefGoogle Scholar
  31. 31.
    A.R. Ghiasvand, S. Hajipour, Talanta 146, 417–422 (2016)CrossRefGoogle Scholar
  32. 32.
    V. Gökmen, H.Z. Şenyuva, J. Chromatogr. A 1120, 194–198 (2006)CrossRefGoogle Scholar
  33. 33.
    J.O. Fernandes, C. Soares, J. Chromatogr. A 1175, 1–6 (2007)CrossRefGoogle Scholar
  34. 34.
    E. Bermudo, E. Moyano, L. Puignou, M. Galceran, Anal. Chim. Acta 559, 207–214 (2006)CrossRefGoogle Scholar
  35. 35.
    E. Bermudo, O. Núñez, L. Puignou, M.T. Galceran, J. Chromatogr. A 1129, 129–134 (2006)CrossRefGoogle Scholar

Copyright information

© Iranian Chemical Society 2019

Authors and Affiliations

  • Arezou Taghvimi
    • 1
  • Samin Hamidi
    • 2
  • Yousef Javadzadeh
    • 3
    • 4
  • Siavoush Dastmalchi
    • 3
    • 4
  • Mahnaz Tabibiazar
    • 5
    Email author
  1. 1.Biotechnology Research Centre and Student Research CommitteeTabriz University of Medical ScienceTabrizIran
  2. 2.Food and Drug Safety Research CentreTabriz University of Medical ScienceTabrizIran
  3. 3.Biotechnology Research Center, Faculty of PharmacyTabriz University of Medical ScienceTabrizIran
  4. 4.Faculty of PharmacyNear East UniversityNicosia, Mersin 10Turkey
  5. 5.Drug Applied Research Center and Department of Food Science and Technology, Faculty of Nutrition and Food ScienceTabriz University of Medical ScienceTabrizIran

Personalised recommendations