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Journal of the Iranian Chemical Society

, Volume 16, Issue 3, pp 449–454 | Cite as

Synthesis, crystal structure and luminescence of two barium(II) compounds: from mono- to bis-tetrazole carboxylic acids

  • Xiao Qing Gu
  • Tian Yu Wu
  • Wan Ting Su
  • Yu Jie Shi
  • Zhi Kang Wang
  • Yan Li
  • Xiao Yi Liu
  • Qiao Yun LiEmail author
  • Gao Wen YangEmail author
Original Paper
  • 15 Downloads

Abstract

Tetrazole carboxylates are acknowledged as bifunctional ligands for the construction of new coordination architectures. Two new coordination compounds, [Ba(atzpa)2(H2O)3]n·2nH2O (1) and [Ba2(dtzpda)(H2O)]n (2) have been prepared by solvothermal reactions of BaCl2·2H2O with Hatzpa or H4dtzpda, respectively (Hatzpa = 5-aminotetrazole-1-propanoic acid, H4dtzpda = 3,3-di(1H-tetrazol-5-yl)pentanedioic acid). The X-ray diffraction results reveal that compound 1 is a linear chain in which atzpa acts as a tridentate ligand to bridge adjacent Ba2+ ions in a µ1,1,3-COO mode. In contrast, compound 2 is a three-dimensional network where dtzpda4− acts as a dode-dentate ligand to bridge various Ba2+ ions. Furthermore, the luminescence of Hatzpa, H4dtzpda, compounds 1 and 2 in the solid state at room temperature were investigated.

Keywords

Hatzpa/H4dtzpda Ba(II) Crystal structure Luminescence 

Notes

Acknowledgements

The authors acknowledge financial support from the Natural Science Foundation of Jiangsu Province (Grant no. BK2012210), the Natural Science Foundation of the Jiangsu Higher Education Institutions of China (Grant no. 10KJB430001) and the Opening Fund of Jiangsu Key Laboratory of Advanced Functional Materials (Grant no. 12KFJJ010).

Supplementary material

13738_2018_1515_MOESM1_ESM.cif (22 kb)
Supplementary material 1 (CIF 21 KB)
13738_2018_1515_MOESM2_ESM.pdf (205 kb)
Supplementary material 2 (PDF 205 KB)
13738_2018_1515_MOESM3_ESM.cif (18 kb)
Supplementary material 3 (CIF 18 KB)
13738_2018_1515_MOESM4_ESM.pdf (311 kb)
Supplementary material 4 (PDF 310 KB)
13738_2018_1515_MOESM5_ESM.doc (260 kb)
Supplementary material 5 (DOC 260 KB)

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Copyright information

© Iranian Chemical Society 2018

Authors and Affiliations

  • Xiao Qing Gu
    • 1
  • Tian Yu Wu
    • 1
  • Wan Ting Su
    • 1
  • Yu Jie Shi
    • 1
  • Zhi Kang Wang
    • 1
  • Yan Li
    • 1
  • Xiao Yi Liu
    • 1
  • Qiao Yun Li
    • 1
    Email author
  • Gao Wen Yang
    • 1
    Email author
  1. 1.Jiangsu Laboratory of Advanced Functional Material, Department of Chemistry and Material EngineeringChangshu Institute of TechnologyChangshuPeople’s Republic of China

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