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Magnetic Molecularly Imprinted Polymer Particles Based Micro-Solid Phase Extraction for the Determination of 4-Nitrophenol in Lake Water

  • Aziguli Yigaimu
  • Turghun MuhammadEmail author
  • Wenwu Yang
  • Imran Muhammad
  • Muyasier Wubulikasimu
  • Sergey A. Piletsky
Article
  • 7 Downloads

Abstract

In this work, magnetic molecularly imprinted polymers (MMIPs) were prepared by the method of co-precipitation polymerization on the surface of vinyl-modified silica magnetic particles. Here, 4-nitrophenol (4-NP) was used as a template and vinylimidazole as a functional monomer. The structural features and morphology of MMIPs were characterized by SEM, FT-IR, TEM and XRD techniques. The results showed that the structures of MMIPs have a layer of silica and MIPs on the surface of the Fe3O4 particles, and they could be rapidly separated from the solution using a magnet. MMIPs possess higher adsorption capacity and excellent selectivity towards template (4-NP) than other structural analogues. And it is found to have good imprinting effect. MMIPs were used as micro-solid phase extraction sorbent for selective separation of 4-NP in lake water sample with high recoveries (90.63–95.63%) and low relative standard deviation values (RSD ≤ 3.2%, n = 3).

Keywords

molecularly imprinted polymers magnetic separation micro-solid phase extraction 4-nitrophenol 

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Copyright information

© The Polymer Society of Korea and Springer 2019

Authors and Affiliations

  • Aziguli Yigaimu
    • 1
  • Turghun Muhammad
    • 1
    • 2
    Email author
  • Wenwu Yang
    • 1
  • Imran Muhammad
    • 1
  • Muyasier Wubulikasimu
    • 1
  • Sergey A. Piletsky
    • 3
  1. 1.College of Chemistry & Chemical EngineeringXinjiang University, Xinjiang Key laboratory of Oil and Gas Fine ChemicalsUrumqiP. R. China
  2. 2.State Key Laboratory of Fine ChemicalsDalian University of TechnologyDalianP. R. China
  3. 3.University of Leicester, Department of ChemistryLeicesterUK

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