Investigation on Microstructure, Hardness and Wear Resistance of Electron Beam Wire-Feeding Deposited Inconel 718 Alloy Coatings
- 55 Downloads
Abstract
The Inconel 718 (IN718) alloy coatings were successfully fabricated using electron beam wire-feeding deposition technology. The macrostructure, microstructure and elemental analysis of the deposited coatings were characterized by OM, SEM and EDS. Moreover, the hardness and wear resistance were also investigated experimentally. The results showed that the cross section of the deposited coatings can be divided into three different regions: clad zone (CZ), fusion zone (FZ) and heat affected zone. Equiaxed dendrites appeared in the CZ while columnar dendrites occurred in the FZ, and discrete fine Laves phase particles were formed under low beam current while continuous coarse Laves phase particles were found under high beam current. The EDS results showed that the degree of Nb segregation in FZ is higher than that in CZ. More importantly, the microstructure coarsened and the degree of Nb segregation increased with the increase of beam current. The deposited coating under the lowest beam current (10 mA) has the highest hardness (263 HV0.2) and the minimum specific wear rate (3.95391 × 10−15 m3/Nm), which is corresponding to the fine microstructure, discrete Laves phase particles and low degree of Nb segregation under low beam current.
Graphic Abstract
Keywords
Wire-feeding deposition Electron beam IN718 coating Hardness Wear resistanceNotes
Acknowledgements
This work was supported by the Opening Fund Project (Grant No. kfjj20180610) of Postgraduate Innovation Laboratory of Nanjing University of Aeronautics and Astronautics.
Compliance with Ethical Standards
Conflict of interest
The authors declare no conflict of interest.
References
- 1.M.A. Zaeem, A.J. Clarke, Rapid solidification and phase transformations in additive manufactured materials. JOM 68(3), 928–929 (2016)CrossRefGoogle Scholar
- 2.K. Eimann, M. Drach, K. Wissenbach, A. Gasser, Proceedings of Stuttgarter Lasertage, Stuttgart, Germany (2003)Google Scholar
- 3.A. Gasser, K. Wissenbach, R. Poprawe, Massgeschneiderte Oberflachen durch Laserstrahl-Oberflachenbehandlung mit Zusatzwerkstoffen-eine Ubersicht. Laser und Optoelektron 29(3), 66–75 (1997)Google Scholar
- 4.X. Zhang, W. Li, X. Chen, W. Cui, F. Liou, Evaluation of component repair using direct metal deposition from scanned data. Int. J. Adv. Manuf. Technol. 95(9–12), 3335–3348 (2018)CrossRefGoogle Scholar
- 5.Y. Li, S. Dong, P. He, S. Yan, E. Li, X. Liu, B. Xu, Microstructure characteristics and mechanical properties of new-type FeNiCr laser cladding alloy coating on nodular cast iron. J. Mater. Process. Technol. 269, 163–171 (2019)CrossRefGoogle Scholar
- 6.J. Shi, S.Q. Bai, Research on gear repairing technology by laser cladding. Key Eng. Mater. 546, 40–44 (2013)CrossRefGoogle Scholar
- 7.D. Bartkowski, A. Młynarczak, A. Piasecki, B. Dudziak, M. Gościański, A. Bartkowska, Microstructure, microhardness and corrosion resistance of Stellite-6 coatings reinforced with WC particles using laser cladding. Opt. Laser Technol. 68, 191–201 (2015)CrossRefGoogle Scholar
- 8.D. Verdi, M.A. Garrido, C.J. Múnez, P. Poza, Mechanical properties of Inconel 625 laser cladded coatings: depth sensing indentation analysis. Mater. Sci. Eng. A 598, 15–21 (2014)CrossRefGoogle Scholar
- 9.Z. Zhang, P. Farahmand, R. Kovacevic, Laser cladding of 420 stainless steel with molybdenum on mild steel A36 by a high power direct diode laser. Mater. Des. 109, 686–699 (2016)CrossRefGoogle Scholar
- 10.S.H. Mok, G. Bi, J. Folkes, I. Pashby, Deposition of Ti–6Al–4V using a high power diode laser and wire, part I: investigation on the process characteristics. Surf. Coat. Technol. 202(16), 3933–3939 (2008)CrossRefGoogle Scholar
- 11.I.R. Pashby, S.H. Mok, J. Folkes, 23rd International Congress on Applications of Lasers and Electro-optics, San Francisco, USA (2004), p. 18Google Scholar
- 12.C. Ader, M. Brosemer, C. Freyer, H. Fricke, D. Hennings, F. Klocke, V. Kühne, W. Meiners, C. Over, H. Pleteit, S. Stührmann, I. Wirth, T. Wirtz, K. Wissenbach, Solid Freeform Fabrication Symposium, Austin, TX, USA (2004), p. 26Google Scholar
- 13.H.B. Suo, Z.Y. Chen, J.R. Liu, S.L. Gong, J.Z. Xiao, Microstructure and mechanical properties of Ti–6Al–4V by electron beam rapid manufacturing. Rare Met. Mater. Eng. 43(4), 780–785 (2014)CrossRefGoogle Scholar
- 14.J. Gocke, J. Beuth, K. Taminger, Integrated control of solidification microstructure and melt pool dimensions in electron beam wire feed additive manufacturing of Ti–6Al–4V. Addit. Manuf. 1, 119–126 (2014)CrossRefGoogle Scholar
- 15.R.W. Bush, C.A. Brice, Elevated temperature characterization of electron beam freeform fabricated Ti–6Al–4V and dispersion strengthened Ti–8Al–1Er. Mater. Sci. Eng. A 554, 12–21 (2012)CrossRefGoogle Scholar
- 16.K. Taminger, R.A. Hafley, Electron beam freeform fabrication: a rapid metal deposition process, in Proceedings of the 3rd Annual Automotive Composites Conference (Society of Plastics Engineers, Troy, 2003)Google Scholar
- 17.K.M. Taminger, R.A. Hafley, Electron Beam Freeform Fabrication (EBF3) for Cost Effective Near-Net Shape Manufacturing. NASA Technical Memorandum TM-2006-214284Google Scholar
- 18.C. Körner, Additive manufacturing of metallic components by selective electron beam melting—a review. Int. Mater. Rev. 61(5), 361–377 (2016)CrossRefGoogle Scholar
- 19.M. Anderson, R. Patwa, Y.C. Shin, Laser-assisted machining of Inconel 718 with an economic analysis. Int. J. Mach. Tool Manuf. 46(14), 1879–1891 (2006)CrossRefGoogle Scholar
- 20.K.H. Song, K. Nakata, Microstructural and mechanical properties of friction-stir-welded and post-heat-treated Inconel 718 alloy. J. Alloys Compd. 505(1), 144–150 (2010)CrossRefGoogle Scholar
- 21.Q. Jia, D. Gu, Selective laser melting additive manufactured Inconel 718 superalloy parts: high-temperature oxidation property and its mechanisms. Opt. Laser Technol. 62, 161–171 (2014)CrossRefGoogle Scholar
- 22.M.M. Kirka, K.A. Unocic, N. Raghavan, F. Medina, R.R. Dehoff, S.S. Babu, Microstructure development in electron beam-melted Inconel 718 and associated tensile properties. JOM 68(3), 1012–1020 (2016)CrossRefGoogle Scholar
- 23.S. Sui, H. Tan, J. Chen, C. Zhong, Z. Li, W. Fan, A. Gasser, W. Huang, The influence of Laves phases on the room temperature tensile properties of Inconel 718 fabricated by powder feeding laser additive manufacturing. Acta Mater. 164, 413–427 (2018)CrossRefGoogle Scholar
- 24.R.K. Bird, J. Hibberd, Tensile Properties and Microstructure of Inconel 718 Fabricated with Electron Beam Freeform Fabrication (EBF3). NASA Technical Memorandum TM-2009-215929Google Scholar
- 25.Z. Qiu, P. Zhang, D. Wei, B. Duan, P. Zhou, Tribological behavior of CrCoNiAlTiY coating synthesized by double-glow plasma surface alloying technique. Tribol. Int. 92, 512–518 (2015)CrossRefGoogle Scholar
- 26.Y. Zhang, J. Huang, P. Nie, H. Liu, Z. Li, Y. Wu, An investigation on high power diode laser cladding of Ni–Fe–Cr based alloy coatings. Rare Met. Mater. Eng. 41, 199–202 (2012)CrossRefGoogle Scholar
- 27.P.K. Farayibi, T.E. Abioye, A.T. Clare, A parametric study on laser cladding of Ti–6Al–4V wire and WC/W2C powder. Int. J. Adv. Manuf. Technol. 87(9–12), 3349–3358 (2016)CrossRefGoogle Scholar
- 28.A. Mohammad, A. Alahmari, M. Mohammed, R. Renganayagalu, K. Moiduddin, Effect of energy input on microstructure and mechanical properties of titanium aluminide alloy fabricated by the additive manufacturing process of electron beam melting. Materials 10(2), 211 (2017)CrossRefGoogle Scholar
- 29.Z.G. Gao, O.A. Ojo, Modeling analysis of hybrid laser-arc welding of single-crystal nickel-base superalloys. Acta Mater. 60(6–7), 3153–3167 (2012)CrossRefGoogle Scholar
- 30.K. Moussaoui, W. Rubio, M. Mousseigne, T. Sultan, F. Rezai, Effects of selective laser melting additive manufacturing parameters of Inconel 718 on porosity, microstructure and mechanical properties. Mater. Sci. Eng. A 735, 182–190 (2018)CrossRefGoogle Scholar
- 31.P. Nie, O.A. Ojo, Z. Li, Numerical modeling of microstructure evolution during laser additive manufacturing of a nickel-based superalloy. Acta Mater. 77, 85–95 (2014)CrossRefGoogle Scholar
- 32.C.W. White, M.J. Aziz, Energy deposition, heat flow, and rapid solidification during laser and electron beam irradiation of materials, in Surface Alloying by Ion, Electron, and Laser Beams (American Society for Metals, Metals Park, 1986), pp. 19–50Google Scholar
- 33.H. Qi, M. Azer, A. Ritter, Studies of standard heat treatment effects on microstructure and mechanical properties of laser net shape manufactured INCONEL 718. Metall. Mater. Trans. A 40(10), 2410–2422 (2009)CrossRefGoogle Scholar
- 34.Y.C. Zhang, Z.G. Li, P.L. Nie, Y.X. Wu, Effect of heat treatment on niobium segregation of laser-cladded IN718 alloy coating. Metall. Mater. Trans. A 44(2), 708–716 (2013)CrossRefGoogle Scholar
- 35.K.D. Ramkumar, R.J. Sai, V.S. Reddy, S. Gundla, T.H. Mohan, V. Saxena, N. Arivazhagan, Effect of filler wires and direct ageing on the microstructure and mechanical properties in the multi-pass welding of Inconel 718. J. Manuf. Process. 18, 23–45 (2015)CrossRefGoogle Scholar
- 36.J. Lambarri, J. Leunda, V.G. Navas, C. Soriano, C. Sanz, Microstructural and tensile characterization of Inconel 718 laser coatings for aeronautic components. Opt. Lasers Eng. 51(7), 813–821 (2013)CrossRefGoogle Scholar
- 37.Y.T. Long, P.L. Nie, Z.G. Li, J. Huang, L.I. Xiang, X.M. Xu, Segregation of niobium in laser cladding Inconel 718 superalloy. Trans. Nonferr. Met. Soc. China 26(2), 431–436 (2016)CrossRefGoogle Scholar
- 38.T. Antonsson, H. Fredriksson, The effect of cooling rate on the solidification of Inconel 718. Metall. Mater. Trans. B 36(1), 85–96 (2005)CrossRefGoogle Scholar
- 39.S.G.K. Manikandan, D. Sivakumar, K.P. Rao, M. Kamaraj, Effect of weld cooling rate on Laves phase formation in Inconel 718 fusion zone. J. Mater. Process. Technol. 214(2), 358–364 (2014)CrossRefGoogle Scholar
- 40.H. Xiao, S.M. Li, W.J. Xiao, Y.Q. Li, L.M. Cha, J. Mazumder, L.J. Song, Effects of laser modes on Nb segregation and Laves phase formation during laser additive manufacturing of nickel-based superalloy. Mater. Lett. 188, 260–262 (2016)CrossRefGoogle Scholar
- 41.Y. Zhang, L. Yang, J. Dai, J. Liu, W. Zhang, H. Chen, Z. Wang, K. Shi, Microstructure and mechanical properties of pulsed laser cladded IN718 alloy coating. Surf. Eng. 34(4), 259–266 (2018)CrossRefGoogle Scholar
- 42.C. Cai, B. Song, C.L. Qiu, L.F. Li, P.J. Xue, Q.S. Wei, J.X. Zhou, H. Nan, H.X. Chen, Y.S. Shi, Hot isostatic pressing of in situ TiB/Ti–6Al–4V composites with novel reinforcement architecture, enhanced hardness and elevated tribological properties. J. Alloys Compd. 710, 364–374 (2017)CrossRefGoogle Scholar
- 43.J.B. Cheng, X.B. Liang, Z.H. Wang, B.S. Xu, Dry sliding friction and wear properties of metallic glass coating and martensite stainless coating. Tribol. Int. 60, 140–146 (2013)CrossRefGoogle Scholar
- 44.H. Yang, Y. Liu, T. Zhang, H. Wang, B. Tang, J. Qiao, Dry sliding tribological properties of a dendrite-reinforced Zr-based bulk metallic glass matrix composite. J. Mater. Sci. Technol. 30(6), 576–583 (2014)CrossRefGoogle Scholar
- 45.P.K. Farayibi, Laser Cladding of Ti–6Al–4V with Carbide and Boride Reinforcements Using Wire and Powder Feedstock, PhD thesis (University of Nottingham, Nottingham, 2014)Google Scholar
- 46.L.L. Guo, L. Qin, F.Y. Kong, H. Yi, B. Tang, Improving tribological properties of Ti–5Zr–3Sn–5Mo–15Nb alloy by double glow plasma surface alloying. Appl. Surf. Sci. 388, 203–211 (2016)CrossRefGoogle Scholar
- 47.X.W. Tao, Z.J. Yao, X.X. Luo, Comparison of tribological and corrosion behaviors of Cp Ti coated with the TiO2/graphite coating and nitrided TiO2/graphite coating. J. Alloys Compd. 718, 126–133 (2017)CrossRefGoogle Scholar
- 48.S. Bruschi, R. Bertolini, A. Ghiotti, Coupling machining and heat treatment to enhance the wear behaviour of an additive manufactured Ti6Al4V titanium alloy. Tribol. Int. 116, 58–68 (2017)CrossRefGoogle Scholar
- 49.F.H. Stott, J. Glascott, G.C. Wood, The sliding wear of commercial Fe–12% Cr alloys at high temperature. Wear 101(4), 311–324 (1985)CrossRefGoogle Scholar