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Microstructure and texture development in a polycrystal and different aluminium single crystals subjected to hydrostatic extrusion

  • D Moszczyńska
  • B Adamczyk-CieślakEmail author
  • B Osiak
  • R Lipiec
  • M Kulczyk
  • J Mizera
Article

Abstract

A hydrostatic extrusion (HE) process was applied to commercial pure polycrystalline aluminium (99.9%) and two aluminium single crystals \(\langle {111}\rangle \) and \(\langle {110}\rangle \). On comparison, the results obtained from single crystals and polycrystalline aggregates are unique. Microstructure and crystallographic texture investigations were performed by transmission electron microscopy, electron backscatter diffraction and X-ray diffraction (XRD). Significant differences in grain refinement and texture formation were noticed depending on the starting orientation. The deformed single crystal with \(\langle {110}\rangle \) starting orientation features an average grain size value of 150% higher than the second investigated single crystal (\(0.5\ \upmu \hbox {m}\) for the \(\langle {111}\rangle \) single crystal and \(1.3\ \upmu \hbox {m}\) for the second crystal). In turn, the average grain size obtained for polycrystalline aluminium is \(0.9\ \upmu \hbox {m}\). The deformation process causes a difference in the grain sizes, while a fraction of the high angle grain boundaries have a comparable volume percentage in all the deformed microstructures—reached about 35%. The qualitative and quantitative XRD texture results proved that the HE process leads to the formation of a characteristic fibrous texture.

Keywords

Deformation texture crystallographic orientation single crystal electron backscattering diffraction aluminium 

Notes

Acknowledgements

This work was supported by the National Science Centre in Poland, Project No: 2013/09/B/ST8/03754.

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Copyright information

© Indian Academy of Sciences 2019

Authors and Affiliations

  • D Moszczyńska
    • 1
  • B Adamczyk-Cieślak
    • 1
    Email author
  • B Osiak
    • 1
  • R Lipiec
    • 1
  • M Kulczyk
    • 2
  • J Mizera
    • 1
  1. 1.Faculty of Materials Science and EngineeringWarsaw University of TechnologyWarsawPoland
  2. 2.Institute of High Pressure Physics (Unipress)Polish Academy of SciencesWarsawPoland

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