Journal of Failure Analysis and Prevention

, Volume 16, Issue 3, pp 400–409 | Cite as

Zinc Vapor Trapping Using Copper-Based Materials

Technical Article---Peer-Reviewed

Abstract

As part of the development of a long range solution for zinc vapor capture, a series of experiments utilizing commercially available copper and bronze screen and bronze sheet materials were conducted. The testing used a high-vacuum system in which zinc was vaporized and condensed on the zinc getter material at various temperatures. A fixed zinc vaporization temperature was used and the zinc getter material, and consequently the condensation temperature, was varied. The testing revealed that zinc vapor was captured over a wider range of temperatures on bronze materials than on the copper screens.

Keywords

Zinc Reactions Vapor phase Alloying 

Notes

Acknowledgments

The author would like to acknowledge Katelyn Kessinger, Jonathon Baker, and Craig Stripling for support in fabricating and operating the zinc deposition apparatus. Thanks are also accorded to Tony Curtis and Mary Anton for providing SEM analysis and microscopy support. Finally, the financial support of the Tritium Facility is greatly appreciated in support of this work for the Department of Energy under Contract DE-AC09-08SR22470.

References

  1. 1.
    P.S. Korinko, M.H. Tosten, Analysis of zinc 65 contamination after vacuum thermal process. J. Pract. Fail. Anal. 13(4), 389–395 (2013)CrossRefGoogle Scholar
  2. 2.
    P.S. Korinko, A.J. Duncan, K.J. Stoner, Methods of preventing the spread of zinc contamination during vacuum processing. J. Pract. Fail. Anal. Prev. 14(1), 113–121 (2013)CrossRefGoogle Scholar
  3. 3.
    P.S. Korinko, Zinc Mitigation Interim Report—Thermodynamic Study, Report SRNL-STI-2010-00473, Department of Energy—Office of Science and Technology Information. http://www.osti.gov/scitech/. Accessed 17 Dec 2010
  4. 4.
    P.S. Korinko, Zinc 65 Sequestration Path Forward, Unpublished Memo, SRNL-L4410-2013-00004, Feb. 2013Google Scholar

Copyright information

© ASM International 2016

Authors and Affiliations

  1. 1.Savannah River National Laboratory, Materials Science and TechnologyAikenUSA

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