Advertisement

Russian Chemical Bulletin

, Volume 67, Issue 10, pp 1899–1902 | Cite as

Synthesis of fluorine-containing esters of 2,5-furandicarboxylic acid

  • A. M. Sakharov
  • O. U. Smirnova
  • A. A. Glazkov
  • A. A. Yarosh
Article
  • 11 Downloads

Abstract

Fluorinated esters of 2,5-furandicarboxylic acid have been synthesized starting from 2,5-furan dicarboxylic acid dichloride and fluorine-containing diols. The reaction control was performed by means of 1H, 19F NMR, and IR-spectroscopy. Thermal stability, as well as glass transition temperature, and intrinsic viscosity parameters of the obtained oligomers have been determined.

Key words

2,5-furandicarboxylic acid dichloride polyfluorinated diols fluorine-containing esters of 2,5-furandicarboxylic acid fluorine-containing oligomers intrinsic viscosity TGA DSC NMR- and IR-spectroscopy 

Preview

Unable to display preview. Download preview PDF.

Unable to display preview. Download preview PDF.

References

  1. 1.
    O. Smirnova, A. Glazkov, A. Yarosh, A. Sakharov, Molecules, 2016, 21,904.CrossRefGoogle Scholar
  2. 2.
    R. Filler, J. V. Fenner, C. S. Stokers, J. F. O´Brien, M. Hauptschein, J. Am. Chem. Soc., 1953, 75, 2693.CrossRefGoogle Scholar
  3. 3.
    D. B. Kichura, O. V. Yugach, Khim. Prom-st [Chemical Industry], 1975, 7, 19 (in Russian).Google Scholar
  4. 4.
    R.-J. van Putten, J. C. van der Waal, E. de Jong, C. B. Rasrendra, H. J. Heeres, J. G. de Vries, Chem. Rev., 2013, 113, 1499.CrossRefGoogle Scholar
  5. 5.
    A. M. Sakharov, O. U. Smirnova, A. A. Yarosh, Fluorine Notes, 2017, 113,7.Google Scholar
  6. 6.
    J. C. Morales-Huera, A. M. DeIlarduya, S. Munoz-Guerra, Polymer, 2016, 87,148.CrossRefGoogle Scholar
  7. 7.
    E. N. Ushakova, O. V. Konyushko, A. A. Glazkov, S. P. Krukovsky, Russ. Chem. Bull., 1996, 45, 1501.CrossRefGoogle Scholar

Copyright information

© Springer Science+Business Media, LLC, part of Springer Nature 2018

Authors and Affiliations

  • A. M. Sakharov
    • 1
  • O. U. Smirnova
    • 1
  • A. A. Glazkov
    • 1
  • A. A. Yarosh
    • 1
  1. 1.N. D. Zelinsky Institute of Organic ChemistryRussian Academy of SciencesMoscowRussian Federation

Personalised recommendations